1: 63 percent / dicyclohexylcarbodiimide / tetrahydrofuran / 18 h / 20 °C 2: 60 percent / H2 / 10percent Pd/C / ethanol / 3 h / 2585.7 Torr 3: 97 percent / I2, NaHCO3 / ethanol; H2O / 1.5 h / 20 °C 4: 93 percent / H2, sodium acetate / 10percent Pd/C / ethanol / 3 h / 2327.2 Torr 5: 80 percent / trifluoroacetic acid / 0.25 h / 5 °C View Scheme

暂无反应条件数据

sodium hydroxide in dichloromethane pH=8.5 - 8.8; 2 h; Reflux;

1: 69 percent / 1 h / 230 °C 2: 73 percent / phosphorus oxychloride / 0.25 h / Heating View Scheme

potassium hydroxide