L-2-氨基-5-苯基戊酸合成路线 （共 10 条）
反应条件
hydrogen; palladium 10 on activated carbon in methanol T=20°C; 2 h;
参考文献
IRM LLC
Patent: US2004/198780 A1, 2004 ;
Location in patent: Page 23 ;
反应条件
formate dehydrogenase; nicotinamide adenine dinucleotide; ammonium formate T=30°C; 24 h; PheDH;
参考文献
Asano; Yamada; Kato; Yamaguchi; Hibino; Hirai; Kondo
Journal of Organic Chemistry, 1990 , vol. 55, # 21 p. 5567 - 5571
反应条件
hydrogen; palladium on activated charcoal in methanol
参考文献
Chemical Communications, , # 14 p. 1868 - 1870
反应条件
1: 93 percent / tetramethylguanidinium azide / CH2Cl2 / 0 - 20 °C 2: 91 percent / LiOH; aq. H2O2 / tetrahydrofuran / 20 °C 3: H2 / Pd/C / methanol View Scheme
参考文献
Chemical Communications, , # 14 p. 1868 - 1870
反应条件
1: 91 percent / LiOH; aq. H2O2 / tetrahydrofuran / 20 °C 2: H2 / Pd/C / methanol View Scheme
参考文献
Chemical Communications, , # 14 p. 1868 - 1870
反应条件
potassium hydroxide; potassium phosphate buffer; porcine kidney acylase I T=40°C; relative initial rate of hydrolysis, also with Aspergillus acylase I as a catalyst;
参考文献
Journal of the American Chemical Society, , vol. 111, # 16 p. 6354 - 6364
反应条件
1: 1) Mg / THF 2: 93 percent / 10percent HCl, acetic acid / 3 h / 50 °C 3: 98 percent / ammonium formate, formate dehydrogenase, NAD+, buffer (pH 8.5) / 24 h / 30 °C / PheDH View Scheme
参考文献
Journal of Organic Chemistry, , vol. 55, # 21 p. 5567 - 5571
反应条件
1: aq. NaOH / methanol 2: xylene / (enzymatic racemate resolution) View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 49, p. 3280 - 3284
反应条件
1: 93 percent / 10percent HCl, acetic acid / 3 h / 50 °C 2: 98 percent / ammonium formate, formate dehydrogenase, NAD+, buffer (pH 8.5) / 24 h / 30 °C / PheDH View Scheme
参考文献
Journal of Organic Chemistry, , vol. 55, # 21 p. 5567 - 5571
反应条件
in xylene (enzymatic racemate resolution);
参考文献
Bulletin of the Chemical Society of Japan, , vol. 49, p. 3280 - 3284
