ammonia in pentane
stirring at -78°C for 4 h;; filtration, sepn. by distn. in vacuo respectively sublimation of the distillation residue; elem. anal.;;
参考文献
Paciorek, K. J. L.; Masuda, S. R.; Hoferkamp, L. A.; Nakahara, J. H.; Kratzer, R. H.
Inorganic Chemistry, 1991 , vol. 30, p. 577 - 579
