N-(4-溴苯基)苯并噻唑-2-胺合成路线 （共 5 条）
反应条件
hydrogenchloride in 1,4-dioxane; ethanol
T=120°C; 1 h; Microwave irradiation;
参考文献
BEIJING HANMI PHARMACEUTICAL CO., LTD; ZHANG, Bo; YANG, Jun; LIU, Jinming; HUANG, Hai; WU, Yong; TAO, Ran; XU, Jiangcheng; SHEN, Ning; MOON, Sunghwan; KIM, Maengsup
Patent: WO2013/56679 A1, 2013 ;
Location in patent: Page/Page column 29 ;
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dimethyl sulfoxide
T=20°C; 24 h;
参考文献
Wang, Rui; Yang, Wen-Juan; Yue, Liang; Pan, Wei; Zeng, Hong-Yao
Synlett, 2012 , vol. 23, # 11 p. 1643 - 1648
反应条件
in tetrahydrofuran
T=70°C; 4 h;
参考文献
Cee, Victor J.; Downing, Nicholas S.
Tetrahedron Letters, 2006 , vol. 47, # 22 p. 3747 - 3750
反应条件
1: 1 h / Inert atmosphere; Heating
2: 1,4-diaza-bicyclo[2.2.2]octane / dimethyl sulfoxide / 130 °C / Inert atmosphere
View Scheme
参考文献
Wang, Rui; Chen, Zhi; Yue, Liang; Pan, Wei; Zhao, Jun-Jie
Tetrahedron Letters, 2012 , vol. 53, # 34 p. 4529 - 4531
反应条件
1: neat (no solvent)
2: potassium carbonate / water / 10 h / 100 °C / |Green chemistry
View Scheme
参考文献
Rout, Saroj Kumar; Guin, Srimanta; Nath, Jayashree; Patel, Bhisma K.
Green Chemistry, 2012 , vol. 14, # 9 p. 2491 - 2498
