Tolstikova, O. V.; Tolstikov, A. G.; Shmakov, V. S.; Galkin, E. G.; Vyrypaev, E. M.; et al.
Chemistry of Natural Compounds, 1989 , vol. 25, p. 199 - 202
Khimiya Prirodnykh Soedinenii, 1989 , # 2 p. 232 - 236
1: 65 percent / PBr3 / pyridine; diethyl ether / 1.) -30 deg C, 3h, 2.) 12h, 25 deg C
2: 56 percent / sodium azide / 2-ethoxy-ethanol; H2O / 24 h / 90 °C
3: 95 percent / lithium tetrahydroaluminate / diethyl ether / 0.33 h / Ambient temperature
4: 90 percent / benzene / 0.17 h / 25 °C
View Scheme
参考文献
Tolstikova, O. V.; Tolstikov, A. G.; Shmakov, V. S.; Galkin, E. G.; Vyrypaev, E. M.; et al.
Chemistry of Natural Compounds, 1989 , vol. 25, p. 199 - 202
Khimiya Prirodnykh Soedinenii, 1989 , # 2 p. 232 - 236
1: 100 percent / azoisobutyronitrile / 6 h / -20 °C / Irradiation
2: 95 percent / HCl-gas / 12 h
3: 95 percent / LiAlH4 / diethyl ether / 0.33 h / Ambient temperature
4: 65 percent / PBr3 / pyridine; diethyl ether / 1.) -30 deg C, 3h, 2.) 12h, 25 deg C
5: 56 percent / sodium azide / 2-ethoxy-ethanol; H2O / 24 h / 90 °C
6: 95 percent / lithium tetrahydroaluminate / diethyl ether / 0.33 h / Ambient temperature
7: 90 percent / benzene / 0.17 h / 25 °C
View Scheme
参考文献
Tolstikova, O. V.; Tolstikov, A. G.; Shmakov, V. S.; Galkin, E. G.; Vyrypaev, E. M.; et al.
Chemistry of Natural Compounds, 1989 , vol. 25, p. 199 - 202
Khimiya Prirodnykh Soedinenii, 1989 , # 2 p. 232 - 236
1: 95 percent / LiAlH4 / diethyl ether / 0.33 h / Ambient temperature
2: 65 percent / PBr3 / pyridine; diethyl ether / 1.) -30 deg C, 3h, 2.) 12h, 25 deg C
3: 56 percent / sodium azide / 2-ethoxy-ethanol; H2O / 24 h / 90 °C
4: 95 percent / lithium tetrahydroaluminate / diethyl ether / 0.33 h / Ambient temperature
5: 90 percent / benzene / 0.17 h / 25 °C
View Scheme
参考文献
Tolstikova, O. V.; Tolstikov, A. G.; Shmakov, V. S.; Galkin, E. G.; Vyrypaev, E. M.; et al.
Chemistry of Natural Compounds, 1989 , vol. 25, p. 199 - 202
Khimiya Prirodnykh Soedinenii, 1989 , # 2 p. 232 - 236
1: 56 percent / sodium azide / 2-ethoxy-ethanol; H2O / 24 h / 90 °C
2: 95 percent / lithium tetrahydroaluminate / diethyl ether / 0.33 h / Ambient temperature
3: 90 percent / benzene / 0.17 h / 25 °C
View Scheme
参考文献
Tolstikova, O. V.; Tolstikov, A. G.; Shmakov, V. S.; Galkin, E. G.; Vyrypaev, E. M.; et al.
Chemistry of Natural Compounds, 1989 , vol. 25, p. 199 - 202
Khimiya Prirodnykh Soedinenii, 1989 , # 2 p. 232 - 236
1: 95 percent / HCl-gas / 12 h
2: 95 percent / LiAlH4 / diethyl ether / 0.33 h / Ambient temperature
3: 65 percent / PBr3 / pyridine; diethyl ether / 1.) -30 deg C, 3h, 2.) 12h, 25 deg C
4: 56 percent / sodium azide / 2-ethoxy-ethanol; H2O / 24 h / 90 °C
5: 95 percent / lithium tetrahydroaluminate / diethyl ether / 0.33 h / Ambient temperature
6: 90 percent / benzene / 0.17 h / 25 °C
View Scheme
参考文献
Tolstikova, O. V.; Tolstikov, A. G.; Shmakov, V. S.; Galkin, E. G.; Vyrypaev, E. M.; et al.
Chemistry of Natural Compounds, 1989 , vol. 25, p. 199 - 202
Khimiya Prirodnykh Soedinenii, 1989 , # 2 p. 232 - 236
1: 95 percent / lithium tetrahydroaluminate / diethyl ether / 0.33 h / Ambient temperature
2: 90 percent / benzene / 0.17 h / 25 °C
View Scheme
参考文献
Tolstikova, O. V.; Tolstikov, A. G.; Shmakov, V. S.; Galkin, E. G.; Vyrypaev, E. M.; et al.
Chemistry of Natural Compounds, 1989 , vol. 25, p. 199 - 202
Khimiya Prirodnykh Soedinenii, 1989 , # 2 p. 232 - 236
