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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
62787-40-0
合成路线
（共 10 条）
125232-06-6
→
反应条件
62787-40-0
反应条件
T=20°C;
参考文献
Farzipour, Soghra; Saeedi, Mina; Mahdavi, Mohammad; Yavari, Hossein; Mirzahekmati, Mohammadreza; Ghaemi, Nasser; Foroumadi, Alireza; Shafiee, Abbas
Synthetic Communications, 2014 , vol. 44, # 4 p. 481 - 487
552-16-9
邻硝基苯甲酸
→
反应条件
62787-40-0
反应条件
1: PCl5 / a. RT, 20min; b. reflux, 1.5h 2: benzene / 0.75 h / Ambient temperature 3: 55.6 percent / FeSO4*7H2O, NH4OH / H2O / 3 h / Heating 4: 43.7 percent / 6 h / 154 °C View Scheme
参考文献
Joshi; Chaudhari; Mogera
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 5 p. 431 - 434
4230-93-7
3,4-二甲氧基-~-硝基苯乙烯
→
反应条件
62787-40-0
反应条件
1: LAH 2: benzene / 0.75 h / Ambient temperature 3: 55.6 percent / FeSO4*7H2O, NH4OH / H2O / 3 h / Heating 4: 43.7 percent / 6 h / 154 °C View Scheme
参考文献
Joshi; Chaudhari; Mogera
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 5 p. 431 - 434
19007-49-9
→
反应条件
62787-40-0
反应条件
1: 55.6 percent / FeSO4*7H2O, NH4OH / H2O / 3 h / Heating 2: 43.7 percent / 6 h / 154 °C View Scheme
参考文献
Joshi; Chaudhari; Mogera
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 5 p. 431 - 434
121-33-5
香草醛
→
反应条件
62787-40-0
反应条件
3: LAH 4: benzene / 0.75 h / Ambient temperature 5: 55.6 percent / FeSO4*7H2O, NH4OH / H2O / 3 h / Heating 6: 43.7 percent / 6 h / 154 °C View Scheme
参考文献
Joshi; Chaudhari; Mogera
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 5 p. 431 - 434
120-14-9
3,4-二甲氧基苯甲醛
→
反应条件
62787-40-0
反应条件
2: LAH 3: benzene / 0.75 h / Ambient temperature 4: 55.6 percent / FeSO4*7H2O, NH4OH / H2O / 3 h / Heating 5: 43.7 percent / 6 h / 154 °C View Scheme
参考文献
Joshi; Chaudhari; Mogera
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 5 p. 431 - 434
120-20-7
3,4-二甲氧基苯乙胺
→
反应条件
62787-40-0
反应条件
1: benzene / 0.75 h / Ambient temperature 2: 55.6 percent / FeSO4*7H2O, NH4OH / H2O / 3 h / Heating 3: 43.7 percent / 6 h / 154 °C View Scheme
参考文献
Joshi; Chaudhari; Mogera
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 5 p. 431 - 434
610-14-0
2-硝基苯甲酰氯
→
反应条件
62787-40-0
反应条件
1: benzene / 0.75 h / Ambient temperature 2: 55.6 percent / FeSO4*7H2O, NH4OH / H2O / 3 h / Heating 3: 43.7 percent / 6 h / 154 °C View Scheme
参考文献
Joshi; Chaudhari; Mogera
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 5 p. 431 - 434
125232-06-6
+
122-51-0
原甲酸三乙酯
→
反应条件
62787-40-0
反应条件
T=154°C; 6 h;
参考文献
Joshi; Chaudhari; Mogera
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 5 p. 431 - 434
118-48-9
靛红酸酐
+
120-20-7
3,4-二甲氧基苯乙胺
→
反应条件
62787-40-0
反应条件
1: water / 2 h / 20 °C / |Green chemistry 2: 20 °C View Scheme
参考文献
Farzipour, Soghra; Saeedi, Mina; Mahdavi, Mohammad; Yavari, Hossein; Mirzahekmati, Mohammadreza; Ghaemi, Nasser; Foroumadi, Alireza; Shafiee, Abbas
Synthetic Communications, 2014 , vol. 44, # 4 p. 481 - 487
