反应条件
1: triethylamine / 16 h / 20 °C / |Inert atmosphere
2: N-ethyl-N,N-diisopropylamine; methanesulfonyl chloride / dichloromethane / 20 °C / |Inert atmosphere; |Cooling with ice
3: dihydrogen peroxide; sodium hydroxide / methanol / 0.17 h / |Inert atmosphere; |Cooling with ice
4: dichloromethane / 6 h / 20 °C / |Inert atmosphere
5: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 16 h / |Inert atmosphere
View Scheme
参考文献
Agut, Juan; Vidal, Andreu; Rodriguez, Santiago; Gonzalez, Florenci V.
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5717 - 5722