2-(2-氯乙氧基)乙醇合成路线 (共 66 条)
反应条件
in toluene T=40°C; 48 h;
参考文献
Rattay; Rettig
Pharmazie, 1997 , vol. 52, # 9 p. 676 - 679
反应条件
potassium carbonate in acetonitrile
参考文献
Liu, Wujun; Wu, Siguo; Hou, Shuhua; Zhao, Zongbao (Kent)
Tetrahedron, 2009 , vol. 65, # 40 p. 8378 - 8383
反应条件
chlorine in dichloromethane
T=10 - 20°C; 0.25 h; Yield given. Title compound not separated from byproducts;
参考文献
Beger, J.; Poeschmann, C.; Shabanov, A. L.; Gurbanov, P. A.
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 6 p. 996 - 1007
反应条件
2,6-dimethylpyridine
参考文献
Smeets, J. W. H.; Visser, H. C.; Kaats-Richters, V. E. M.; Nolte, R. J. M.
Recueil des Travaux Chimiques des Pays-Bas, 1990 , vol. 109, # 3 p. 147 - 153
反应条件
potassium carbonate in N,N-dimethyl-formamide
Alkylation; 72 h; Heating;
参考文献
Griffin, Jonathan L. W.; Coveney, Peter V.; Whiting, Andrew; Davey, Roger
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 10 p. 1973 - 1981
反应条件
potassium carbonate in N,N-dimethyl-formamide
96 h; Heating;
参考文献
Anelli, Pier Lucio; Montanari, Fernando; Quici, Silvio; Ciani, Gianfranco; Sironi, Angelo
Journal of Organic Chemistry, 1988 , vol. 53, # 22 p. 5292 - 5298
反应条件
Williamson ether synthesis; Inert atmosphere;
参考文献
Liu, Wujun; Wu, Siguo; Hou, Shuhua; Zhao, Zongbao (Kent)
Tetrahedron, 2009 , vol. 65, # 40 p. 8378 - 8383
反应条件
chlorine in dichloromethane
T=10 - 20°C; 0.25 h; Yield given. Title compound not separated from byproducts;
参考文献
Beger, J.; Poeschmann, C.; Shabanov, A. L.; Gurbanov, P. A.
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 6 p. 996 - 1007
反应条件
potassium carbonate; potassium iodide in N,N-dimethyl-formamide
T=100°C; 16 h;
参考文献
Steuerman, David W.; Tseng, Hsian-Rong; Peters, Andrea J.; Flood, Amar H.; Jeppesen, Jan O.; Nielsen, Kent A.; Stoddart, J. Fraser; Heath, James R.
Angewandte Chemie - International Edition, 2004 , vol. 43, # 47 p. 6486 - 6491
参考文献
Lermit; Moggridge
Journal of the Chemical Society, 1947 , p. 530,532