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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
62806-35-3
合成路线
（共 7 条）
141-82-2
丙二酸
+
20005-42-9
5-(4-溴苯基)-2-呋喃甲醛
→
反应条件
62806-35-3
反应条件
piperidine; pyridine 4 h; Heating;
参考文献
Obushak, N. D.; Ganushchak, N. I.; Lesyuk, A. I.; Dzikovskaya, L. M.; Kisilitsa, P. P.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 4 p. 748 - 753
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 4 p. 873 - 880
1899-24-7
5-溴-2-呋喃甲醛
→
反应条件
62806-35-3
反应条件
1: (Ph3P)4Pd; aq. K2CO3 / toluene; ethanol / 5 h / Heating 2: pyridine; piperidine / 2 h / Heating View Scheme
参考文献
Wiesner, Jochen; Mitsch, Andreas; Wissner, Pia; Kraemer, Oliver; Jomaa, Hassan; Schlitzer, Martin
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 19 p. 2681 - 2683
5467-74-3
4-溴苯硼酸
→
反应条件
62806-35-3
反应条件
1: (Ph3P)4Pd; aq. K2CO3 / toluene; ethanol / 5 h / Heating 2: pyridine; piperidine / 2 h / Heating View Scheme
参考文献
Wiesner, Jochen; Mitsch, Andreas; Wissner, Pia; Kraemer, Oliver; Jomaa, Hassan; Schlitzer, Martin
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 19 p. 2681 - 2683
13803-39-9
5-苯基-2-糠醛
→
反应条件
62806-35-3
反应条件
1: toluene / 2 h / Reflux 2: water; potassium hydroxide / 4 h / Reflux View Scheme
参考文献
Paizs, Csaba; Tosa, Monica Ioana; Bencze, Laszlo Csaba; Brem, Juergen; Irimie, Florin Dan; Retey, Janos
Heterocycles, 2011 , vol. 82, # 2 p. 1217 - 1228
176684-12-1
→
反应条件
62806-35-3
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 20 °C / Inert atmosphere 1.2: 20 - 60 °C 2.1: water; sodium hydroxide / methanol / 20 h / 20 °C 3.1: toluene / 2 h / Reflux 4.1: hydrogenchloride / 1,4-dioxane / 4 h / Reflux 5.1: phenylalanine ammonia-lyase / 192 h / 30 °C / pH 8.8 / aq. buffer; Inert atmosphere; Enzymatic reaction View Scheme
参考文献
Paizs, Csaba; Tosa, Monica Ioana; Bencze, Laszlo Csaba; Brem, Juergen; Irimie, Florin Dan; Retey, Janos
Heterocycles, 2011 , vol. 82, # 2 p. 1217 - 1228
33342-28-8
→
反应条件
62806-35-3
反应条件
1.1: thionyl chloride; benzotriazol-1-ol / dichloromethane 2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 20 °C / Inert atmosphere 2.2: 20 - 60 °C 3.1: water; sodium hydroxide / methanol / 20 h / 20 °C 4.1: toluene / 2 h / Reflux 5.1: hydrogenchloride / 1,4-dioxane / 4 h / Reflux 6.1: phenylalanine ammonia-lyase / 192 h / 30 °C / pH 8.8 / aq. buffer; Inert atmosphere; Enzymatic reaction View Scheme
参考文献
Paizs, Csaba; Tosa, Monica Ioana; Bencze, Laszlo Csaba; Brem, Juergen; Irimie, Florin Dan; Retey, Janos
Heterocycles, 2011 , vol. 82, # 2 p. 1217 - 1228
20005-42-9
5-(4-溴苯基)-2-呋喃甲醛
→
反应条件
62806-35-3
反应条件
1.1: sodium tetrahydroborate / methanol / 20 °C 2.1: thionyl chloride; benzotriazol-1-ol / dichloromethane 3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 20 °C / Inert atmosphere 3.2: 20 - 60 °C 4.1: water; sodium hydroxide / methanol / 20 h / 20 °C 5.1: toluene / 2 h / Reflux 6.1: hydrogenchloride / 1,4-dioxane / 4 h / Reflux 7.1: phenylalanine ammonia-lyase / 192 h / 30 °C / pH 8.8 / aq. buffer; Inert atmosphere; Enzymatic reaction View Scheme
参考文献
Paizs, Csaba; Tosa, Monica Ioana; Bencze, Laszlo Csaba; Brem, Juergen; Irimie, Florin Dan; Retey, Janos
Heterocycles, 2011 , vol. 82, # 2 p. 1217 - 1228
