反应条件
1: sulfuric acid / acetone / 48 h
2: 4-(N,N-dimethlyamino)pyridine; pyridine / 5 h / 20 °C / |Cooling with ice; |Inert atmosphere
3: sodium azide / N,N-dimethyl-formamide / 16 h / 120 °C
View Scheme
参考文献
Moreau, Christelle; Kirchberger, Tanja; Swarbrick, Joanna M.; Bartlett, Stephen J.; Fliegert, Ralf; Yorgan, Timur; Bauche, Andreas; Harneit, Angelika; Guse, Andreas H.; Potter, Barry V. L.
Journal of Medicinal Chemistry, 2013 , vol. 56, # 24 p. 10079 - 10102