2-(烯丙氧基)苯甲酸甲酯合成路线 （共 29 条）
反应条件
potassium carbonate in acetone
Heating;
参考文献
Robertson, David W.; Lacefield, William B.; Bloomquist, William; Pfeifer, William; Simon, Richard L.; Cohen, Marlene L.
Journal of Medicinal Chemistry, 1992 , vol. 35, # 2 p. 310 - 319
参考文献
Foeldi
Chemische Berichte, 1920 , vol. 53, p. 1837
Chemische Berichte, 1927 , vol. 60, p. 656,660
反应条件
1: NaOH-solution
2: alcohol
View Scheme
参考文献
Foeldi
Chemische Berichte, 1920 , vol. 53, p. 1837
Chemische Berichte, 1927 , vol. 60, p. 656,660
反应条件
2: sodium methylate
3: 250 °C
4: sodium methylate
5: methanol. NaOH-solution
6: >100
View Scheme
参考文献
Claisen; Eisleb
Justus Liebigs Annalen der Chemie, 1913 , vol. 401, p. 44
反应条件
2: sodium methylate
3: 250 °C
View Scheme
参考文献
Claisen; Eisleb
Justus Liebigs Annalen der Chemie, 1913 , vol. 401, p. 44
反应条件
1: 94 percent / 2 h / 200 °C
View Scheme
参考文献
Stanetty, Peter; Koller, Herbert; Puerstinger, Gerhard
Monatshefte fuer Chemie, 1990 , vol. 121, # 11 p. 883 - 891
反应条件
sodium hydroxide in ethanol
Heating;
参考文献
Shimizu, Tomio; Hayashi, Yoshiyuki; Nagano, Yoshio; Teramura, Kazuhiro
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 2 p. 429 - 434
反应条件
1: 99.8 percent / 15 h / Heating
2: NaH / 1) 20 min at 0 deg C 2) reflux for 12 h
3: NaOH / 1) 1h reflux with NaOH 2) concentrated HCl
4: SOCl2
5: 1) BF3*THF 2) NaOH, 30percent H2O2 / 2) at 55-60 deg C for 90 min
6: 88 percent / triethylamine / CH2Cl2 / 2.5 h / Ambient temperature
7: 100 percent / LiBr / dimethylformamide
8: 80 percent / Mg / tetrahydrofuran / 48 h / Heating
9: 67 percent / 4.5M HCl / 18 h / Heating
View Scheme
参考文献
Meyers, A. I.; Reuman, Michael; Gabel, Richard A.
Journal of Organic Chemistry, 1981 , vol. 46, # 4 p. 783 - 788
反应条件
1: 95 percent / aq. NaOH / aq. ethanol / Heating
2: thionyl chloride
View Scheme
参考文献
Shimizu, Tomio; Hayashi, Yoshiyuki; Nagano, Yoshio; Teramura, Kazuhiro
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 2 p. 429 - 434
