3-(4'-氯苯基)丙醇合成路线 （共 19 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 3 h; Heating;
参考文献
Journal of Medicinal Chemistry, , vol. 45, # 16 p. 3549 - 3557
反应条件
sodium tetrahydroborate T=20°C; 0.25 h;
参考文献
Tetrahedron Letters, , vol. 43, # 9 p. 1657 - 1660
反应条件
palladium 10 on activated carbon; hydrogen in ethyl acetate T=20°C; 12 h;
参考文献
Journal of the Indian Chemical Society, , vol. 90, # 10 p. 1853 - 1860
反应条件
1: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=20°C; 0.5 h; 2: With sodium tetrahydroborate; cerium(III) chloride; water in tetrahydrofuran T=0°C; 0.5 h;
参考文献
Synthesis, , # 9 art. no. M12811SS, p. 1375 - 1382
反应条件
1: diisobutylaluminium hydride / dichloromethane / 3 h / 0 - 20 °C 2: palladium 10 on activated carbon; hydrogen / ethyl acetate / 12 h / 20 °C View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 90, # 10 p. 1853 - 1860
反应条件
(i) Mg, (ii) /BRN= 102378/; Multistep reaction;
参考文献
Journal of the Chemical Society, , p. 1548 - 1553
反应条件
1.1: 62 percent / pyridinium chlorochromate / CH2Cl2 / 20 h / 20 °C 2.1: NH4Cl; aq. NH3 / ethanol / 24 h / 20 °C 2.2: 32 percent / aq. HCl / ethanol / 6 h / Heating View Scheme
参考文献
Nestl, Bettina M.; Glueck, Silvia M.; Hall, Melanie; Kroutil, Wolfgang; Stuermer, Rainer; Hauer, Bernhard; Faber, Kurt
European Journal of Organic Chemistry, 2006 , # 20 p. 4573 - 4577
反应条件
pyridine; chromium(VI) oxide in dichloromethane 0.25 h; Ambient temperature;
参考文献
Goosen, Andre; Marais, Charles F.; McCleland, Cedric W.; Rinaldi, Fabrizio C.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 6 p. 1227 - 1236
反应条件
bis(trichloromethyl) carbonate; triethylamine in dichloromethane Schlenk techniqueInert atmosphere;
参考文献
Gao, Ke; Yoshikai, Naohiko
Journal of the American Chemical Society, 2013 , vol. 135, # 25 p. 9279 - 9282
