2-(3,5-二甲基-1H-吡唑-1-基)乙胺合成路线 (共 5 条)
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in benzene T=75°C; 2 h;
参考文献
Asratyan; Attaryan; Pogosyan; Eliazyan; Darbinyan; Matsoyan
Journal of applied chemistry of the USSR, 1986 , vol. 59, # 6 1 p. 1202 - 1206
反应条件
1: With hydrazine hydrate in methanol 3 h; Heating; 2: With hydrogenchloride in methanol; water Further stages.;
参考文献
Palma, Elisa; Oliveira, Bruno L.; Figueira, Flavio; Correia, Joao D. G.; Raposinho, Paula D.; Santos, Isabel
Journal of Labelled Compounds and Radiopharmaceuticals, 2007 , vol. 50, # 13 p. 1176 - 1184
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in benzene 2 h; Heating;
参考文献
Russian Journal of General Chemistry, , vol. 78, # 1 p. 136 - 138
反应条件
1: 56 percent / acetonitrile / 72 h / Heating 2: 63 percent / hydrazine monohydrate / methanol / 3 h / Heating View Scheme
参考文献
Dalton Transactions, , # 47 p. 5630 - 5640
反应条件
1: 70 percent / dimethylformamide / 1 h / 100 °C 2: 1) 98percent hydrazine hydrate, 2) conc. HCl / 1) ethanol, reflux, 1 h, 2) reflux, 1 h View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 111, # 9 p. 371 - 378