2: 41 percent / n-Bu3SnH, Et3B / benzene; hexane / 0.25 h / 20 °C
View Scheme
参考文献
Nozaki, Kyoko; Oshima, Koichiro; Utimoto, Kiitiro
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, p. 2578 - 2583
→
反应条件
2,6-di-tert-butyl-pyridine; copper(II) bis(trifluoromethanesulfonate) in dichloromethane
T=70°C; 20 h; Inert atmosphere;
参考文献
Phipps, Robert J.; McMurray, Lindsay; Ritter, Stefanie; Duong, Hung A.; Gaunt, Matthew J.
Journal of the American Chemical Society, 2012 , vol. 134, # 26 p. 10773 - 10776
1: 74 percent / m-chloroperbenzoic acid / CH2Cl2 / 5 h / 0 °C
2: 2.8M Me2AlCl,hexane / CH2Cl2 / -78 - -10 °C
View Scheme
参考文献
Fleming, Ian; Newton, Trevor W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 119 - 124
