1-溴-3-邻苯二甲酰亚氨基-2-丙烷酮合成路线 （共 13 条）
反应条件
1: acetic acid
2: sulfuryl dichloride
View Scheme
参考文献
Yang, Yajun; Feng, Ziming; Jiang, Jianshuang; Yang, Yanan; Pan, Xiandao; Zhang, Peicheng
Chemical and Pharmaceutical Bulletin, 2011 , vol. 59, # 8 p. 1016 - 1019
反应条件
sodium hydrogencarbonate in N,N-dimethyl acetamide
1.) RT, 24 h, 2.) 40 deg C, 2 h;
参考文献
Temple, Carroll; Wheeler, Glynn P.; Elliott, Robert D.; Rose, Jerry D.; Kussner, Conrad L.; et al.
Journal of Medicinal Chemistry, 1982 , vol. 25, # 9 p. 1045 - 1050
反应条件
1: dimethylformamide; sodium ethylate
2: hydrobromic acid; water
3: 170 °C / 3 - 4 Torr
View Scheme
参考文献
Tschudy; Collins
Journal of Organic Chemistry, 1959 , vol. 24, p. 556
