您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
62856-05-7
合成路线
（共 6 条）
589-87-7
对溴碘苯
+
88020-03-5
→
反应条件
62856-05-7
反应条件
piperidine; copper(l) iodide; triphenylphosphine; trans-dichlorobis(triphenylphosphine)palladium(II) T=20°C; Sonogashira coupling reaction; 3 h;
参考文献
Ito, Shunji; Wehmeier, Mike; Diedrich Brand; Kuebel, Christian; Epsch, Rebekka; Rabe, Juergen P.; Muellen, Klaus
Chemistry - A European Journal, 2000 , vol. 6, # 23 p. 4327 - 4342
108-86-1
溴代苯
→
反应条件
62856-05-7
反应条件
1: 67 percent / AlCl3 / 1 h / 50 °C 2: 68 percent / hydrazine hydrate; KOH / triethylene glycol / 2 h / 210 °C 3: 89 percent / PPh3; copper iodide; piperidine / trans-dichlorobis(triphenylphosphine)palladium(II) / 24 h / 80 °C 4: 95 percent / aq. KF / dimethylformamide / 3 h / 20 °C 5: 74 percent / PPh3; copper iodide; piperidine / trans-dichlorobis(triphenylphosphine)palladium(II) / 3 h / 20 °C View Scheme
参考文献
Ito, Shunji; Wehmeier, Mike; Diedrich Brand; Kuebel, Christian; Epsch, Rebekka; Rabe, Juergen P.; Muellen, Klaus
Chemistry - A European Journal, 2000 , vol. 6, # 23 p. 4327 - 4342
112-16-3
月桂酰氯
→
反应条件
62856-05-7
反应条件
1: 67 percent / AlCl3 / 1 h / 50 °C 2: 68 percent / hydrazine hydrate; KOH / triethylene glycol / 2 h / 210 °C 3: 89 percent / PPh3; copper iodide; piperidine / trans-dichlorobis(triphenylphosphine)palladium(II) / 24 h / 80 °C 4: 95 percent / aq. KF / dimethylformamide / 3 h / 20 °C 5: 74 percent / PPh3; copper iodide; piperidine / trans-dichlorobis(triphenylphosphine)palladium(II) / 3 h / 20 °C View Scheme
参考文献
Ito, Shunji; Wehmeier, Mike; Diedrich Brand; Kuebel, Christian; Epsch, Rebekka; Rabe, Juergen P.; Muellen, Klaus
Chemistry - A European Journal, 2000 , vol. 6, # 23 p. 4327 - 4342
126930-72-1
1-溴-4-十二烷基苯
→
反应条件
62856-05-7
反应条件
1: 89 percent / PPh3; copper iodide; piperidine / trans-dichlorobis(triphenylphosphine)palladium(II) / 24 h / 80 °C 2: 95 percent / aq. KF / dimethylformamide / 3 h / 20 °C 3: 74 percent / PPh3; copper iodide; piperidine / trans-dichlorobis(triphenylphosphine)palladium(II) / 3 h / 20 °C View Scheme
参考文献
Ito, Shunji; Wehmeier, Mike; Diedrich Brand; Kuebel, Christian; Epsch, Rebekka; Rabe, Juergen P.; Muellen, Klaus
Chemistry - A European Journal, 2000 , vol. 6, # 23 p. 4327 - 4342
231606-35-2
→
反应条件
62856-05-7
反应条件
1: 68 percent / hydrazine hydrate; KOH / triethylene glycol / 2 h / 210 °C 2: 89 percent / PPh3; copper iodide; piperidine / trans-dichlorobis(triphenylphosphine)palladium(II) / 24 h / 80 °C 3: 95 percent / aq. KF / dimethylformamide / 3 h / 20 °C 4: 74 percent / PPh3; copper iodide; piperidine / trans-dichlorobis(triphenylphosphine)palladium(II) / 3 h / 20 °C View Scheme
参考文献
Ito, Shunji; Wehmeier, Mike; Diedrich Brand; Kuebel, Christian; Epsch, Rebekka; Rabe, Juergen P.; Muellen, Klaus
Chemistry - A European Journal, 2000 , vol. 6, # 23 p. 4327 - 4342
170698-87-0
→
反应条件
62856-05-7
反应条件
1: 95 percent / aq. KF / dimethylformamide / 3 h / 20 °C 2: 74 percent / PPh3; copper iodide; piperidine / trans-dichlorobis(triphenylphosphine)palladium(II) / 3 h / 20 °C View Scheme
参考文献
Ito, Shunji; Wehmeier, Mike; Diedrich Brand; Kuebel, Christian; Epsch, Rebekka; Rabe, Juergen P.; Muellen, Klaus
Chemistry - A European Journal, 2000 , vol. 6, # 23 p. 4327 - 4342
