2,3-二溴-3-苯基丙酸合成路线 (共 90 条)
参考文献
Paulson; MacGregor
Journal of the American Chemical Society, 1951 , vol. 73, p. 679
反应条件
1: ethanolic KOH-solution 2: sulfuric acid 3: aqueous ethanol View Scheme
参考文献
Gitsels; Wibaut
Recueil des Travaux Chimiques des Pays-Bas, 1940 , vol. 59, p. 1093,1100
反应条件
1: natrium carbonate 2: potassium hydroxide; absolute alcohol / 130 - 135 °C 3: alcoholic potash / 130 - 140 °C View Scheme
参考文献
Nef
Justus Liebigs Annalen der Chemie, 1899 , vol. 308, p. 325
反应条件
1: thionyl chloride / Heating 2: 74 percent / pyridine / benzene / 3 h 3: 63 percent / conc. sulphuric acid / 0.25 h / 95 °C 4: 69 percent / triethylamine / CHCl3 / 0.5 h / Heating View Scheme
参考文献
Natarajan, M.; Manimaran, T.; Ramakrishnan, V. T.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 6 p. 529 - 534
反应条件
1: natrium carbonate 2: diethyl ether; sodium 3: absolute diethyl ether View Scheme
参考文献
Nef
Justus Liebigs Annalen der Chemie, 1899 , vol. 308, p. 325
反应条件
indium; CoCl2.6H2O in methanol T=20°C; 0.5 h; chemoselective reaction;
参考文献
Yanada, Reiko; Bessho, Kiyoshi; Yanada, Kazuo
Chemistry Letters, 1994 , # 7 p. 1279 - 1282
反应条件
aluminium; nickel dichloride in tetrahydrofuran Dehalogenation;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 36, # 6 p. 528 - 529
反应条件
dimethyl sulfoxide T=100°C; 1 h;
参考文献
Li, Wei; Li, Jianchang; Lin, Melissa; Wacharasindhu, Sumrit; Tabei, Keiko; Mansour, Tarek S.
Journal of Organic Chemistry, 2007 , vol. 72, # 16 p. 6016 - 6021
参考文献
Pfeiffer
Chemische Berichte, 1910 , vol. 43, p. 3044
Chemische Berichte, 1915 , vol. 48, p. 1053
参考文献
Paulson; MacGregor
Journal of the American Chemical Society, 1951 , vol. 73, p. 679