2,5-二甲氧酰基-1,4-环己二酮合成路线 （共 24 条）
反应条件
sodium methylate in methanol 20 h;
参考文献
Seebach, Dieter; Hoffmann, Torsten; Kuehnle, Florian N. M.; Kinkel, Joachim N.; Schulte, Michael
Helvetica Chimica Acta, 1995 , vol. 78, # 6 p. 1525 - 1540
反应条件
potassium iodide in N,N-dimethyl-formamide T=20°C; Condensation; esterification; cyclisation; 5 h;
参考文献
Segat-Dioury, Fabienne; Lingibe, Olivier; Graffe, Bernadette; Sacquet, Marie-Claude; Lhommet, Gerard
Tetrahedron, 2000 , vol. 56, # 2 p. 233 - 248
反应条件
1: bromine / 0.5 h 2: potassium carbonate / ethanol View Scheme
参考文献
Asian Journal of Chemistry, , vol. 25, # 3 p. 1349 - 1352
反应条件
potassium carbonate in ethanol
参考文献
Asian Journal of Chemistry, , vol. 25, # 3 p. 1349 - 1352
反应条件
sodium T=90 - 100°C;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 404, p. 299
反应条件
in N,N-dimethyl-formamide Ambient temperature;
参考文献
Heterocycles, , vol. 45, # 8 p. 1451 - 1455
反应条件
bei laengerem Erhitzen;
参考文献
Monatshefte fuer Chemie, , vol. 32, p. 77
反应条件
1: With phosphoric acid T=20 - 100°C; 4 h; 2: With sodium hydroxide; m-nitrobenzene sulfonic acid sodium salt in water 4 h; Heating / reflux; 3: With sulfuric acid pH=3; Product distribution / selectivity;
参考文献
MCA TECHNOLOGIES GMBH
Patent: WO2005/85364 A1, 2005 ;
Location in patent: Page/Page column 16 ;
反应条件
hydrogenchloride; potassium hydroxide in ethanol; water; acetic acid
参考文献
Bayer Aktiengesellschaft
Patent: US4981997 A1, 1991 ;
反应条件
hydrogenchloride; potassium hydroxide in ethanol; water; acetic acid
参考文献
Bayer Aktiengesellschaft
Patent: US4981997 A1, 1991 ;
