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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-辛炔
合成路线
（共 595 条）
629-05-0
1-辛炔
+
105090-58-2
→
反应条件
19447-29-1
2-壬炔
+
37011-94-2
7-十四碳炔-1-醇
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Brown, Herbert C.; Basavaiah, D.; Bhat, N. G.
Journal of Organic Chemistry, 1986 , vol. 51, # 24 p. 4518 - 4521
629-05-0
1-辛炔
+
6630-33-7
邻溴苯甲醛
→
反应条件
107586-15-2
2-辛炔-1-苯甲醛
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide in triethylamine T=65°C; Sonogashira coupling; 16 h;
参考文献
Hashmi, A. Stephen K.; Buehrle, Miriam; Salathe, Ralph; Bats, Jan W.
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 13 p. 2059 - 2064
629-05-0
1-辛炔
→
反应条件
1072-19-1
1,2-辛二烯
反应条件
1: (i) PCl5, benzene, (ii) H2O 2: aq. NaOH View Scheme
参考文献
Meisters,A.; Swan,J.M.
Australian Journal of Chemistry, 1965 , vol. 18, p. 155 - 162
629-05-0
1-辛炔
→
反应条件
111423-27-9
(S)-(-)-1,1,1-三氟-2-癸醇
反应条件
1: 66 percent / lithium diisopropyl amine / tetrahydrofuran 2: hydrogen / Lindar catalyst / hexane 3: pyridine / CH2Cl2 / 10 h / Ambient temperature 4: 2.) hydrogen / 1.) lipase-MY (Candida cylindracea); 2.) PtO2 / 1.) H2O; 2.) EtOH View Scheme
参考文献
Hanzawa; Kawagoe; Ito; Kobayashi
Chemical and Pharmaceutical Bulletin, 1987 , vol. 35, # 4 p. 1633 - 1636
629-05-0
1-辛炔
+
3248-78-0
→
反应条件
18277-02-6
反应条件
(i) nBuLi, light petroleum, (ii) /BRN= 1776946/, MeSO3H, diglyme, (iii) aq. NaOH, H2O2; Multistep reaction;
参考文献
Pelter,A. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976 , p. 2435 - 2438
629-05-0
1-辛炔
+
108-95-2
苯酚
→
反应条件
18626-98-7
O-(1-甲基庚基)苯酚
+
6052-90-0
反应条件
aluminium phenoxide T=130°C; 8 h; var. ratios of reagents, oth. temperature, oth. time, presence of solvent, pressure 1-1.5 MPa.; Product distribution;
参考文献
Kozlikovskii, Ya. B.; Koshchii, V. A.; Butov, S. A.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 9 p. 1713 - 1716
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 9 p. 1930 - 1934
629-05-0
1-辛炔
→
反应条件
18277-20-8
反应条件
1,4-diaza-bicyclo[2.2.2]octane; copper(l) iodide; ethyl bromoacetate; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=20°C;
参考文献
Liu, Yunyun; Wang, Chunping; Wang, Xiaobo; Wan, Jie-Ping
Tetrahedron Letters, 2013 , vol. 54, # 30 p. 3953 - 3955
629-05-0
1-辛炔
+
115-19-5
2-甲基-3-丁炔-2-醇
→
反应条件
5929-72-6
2,7-二甲基-3,5-辛二炔-2,7-二醇
+
18277-20-8
+
158746-88-4
反应条件
copper(l) iodide; ethyl α,α-dibromoacetoacetate; triethylamine in dichloromethane T=20°C; 23 h; Overall yield = 99 percent;
参考文献
Fan, Xiaohui; Li, Na; Shen, Tong; Cui, Xiao-Meng; Lv, Hao; Zhu, Hong-Bo; Guan, Yong-Hong
Tetrahedron, 2014 , vol. 70, # 2 p. 256 - 261
2510-23-8
3-乙炔基吡啶
+
629-05-0
1-辛炔
→
反应条件
18277-20-8
+
1526988-47-5
+
5069-24-9
反应条件
copper(l) iodide; ethyl α,α-dibromoacetoacetate; triethylamine in dichloromethane T=20°C; 23 h; Overall yield = 98 percent;
参考文献
Fan, Xiaohui; Li, Na; Shen, Tong; Cui, Xiao-Meng; Lv, Hao; Zhu, Hong-Bo; Guan, Yong-Hong
Tetrahedron, 2014 , vol. 70, # 2 p. 256 - 261
629-05-0
1-辛炔
→
反应条件
18277-20-8
+
96185-09-0
反应条件
triethylamine; chloroacetone; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in benzene 2 h;
参考文献
Rossi, Renzo; Carpita, Adriano; Bigelli, Clara
Tetrahedron Letters, 1985 , vol. 26, # 4 p. 523 - 526
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