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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-辛炔
合成路线
（共 595 条）
629-05-0
1-辛炔
+
557-40-4
烯丙基醚
→
反应条件
55976-13-1
(4E)-1,4-十一碳二烯
+
151804-37-4
反应条件
Yield given. Multistep reaction;
参考文献
Suzuki, Noriyuki; Kondakov, Denis Y.; Kageyama, Motohiro; Kotora, Martin; Hara, Ryuichiro; Takahashi, Tamotsu
Tetrahedron, 1995 , vol. 51, # 15 p. 4519 - 4540
629-05-0
1-辛炔
+
607-81-8
苄基丙二酸二乙酯
→
反应条件
141344-90-3
反应条件
potassium acetate; manganese triacetate in acetic acid T=70°C;
参考文献
Bergamini, Fabrizio; Gatti, Norberto; Santi, Roberto; Citterio, Attilio; Nicolini, Marco; Sebastiano, Roberto
Journal of Chemical Research, Miniprint, 1993 , # 9 p. 2455 - 2466
629-05-0
1-辛炔
+
607-81-8
苄基丙二酸二乙酯
→
反应条件
141344-90-3
反应条件
manganese triacetate in acetic acid T=70°C; 24 h;
参考文献
Bergamini, Fabrizio; Gatti, Norberto; Santi, Roberto; Citterio, Attilio; Nicolini, Marco; Sebastiano, Roberto
Journal of Chemical Research, Miniprint, 1993 , # 9 p. 2455 - 2466
629-05-0
1-辛炔
+
35761-83-2
→
反应条件
148802-07-7
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine
参考文献
Odedra, Arjan; Wu, Chang-Jung; Madhushaw, Reniguntala J.; Wang, Su-Lein; Liu, Rai-Shung
Journal of the American Chemical Society, 2003 , vol. 125, # 32 p. 9610 - 9611
629-05-0
1-辛炔
+
74592-24-8
→
反应条件
140840-81-9
反应条件
1: anhydrous 1-octyne With n-butyllithium in hexane T=-78°C; 1 h; Inert atmosphere; 2: Cyclopropanone Ethyl Hemiketal Magnesium Iodide With methyl-magnesium iodide in tetrahydrofuran T=0 - 20°C; 12 h; Inert atmosphere;
参考文献
Trost, Barry M.; Xie, Jia; Maulide, Nuno
Journal of the American Chemical Society, 2008 , vol. 130, # 51 p. 17258 - 17259
629-05-0
1-辛炔
+
83817-31-6
→
反应条件
143145-48-6
反应条件
2,2'-azo-bisisobutyronitrile in benzene Heating;
参考文献
Han, Li-Biao; Ishihara, Ken-Ichi; Kambe, Nobuaki; Ogawa, Akiya; Ryu, Ilhyong; Sonoda, Noboru
Journal of the American Chemical Society, 1992 , vol. 114, # 19 p. 7591 - 7592
629-05-0
1-辛炔
→
反应条件
50606-97-8
对辛基苯甲酰氯
反应条件
1: tetrakis(triphenylphosphine) palladium(0); copper(l) iodide; triethylamine / 12 h / 60 °C / |Inert atmosphere 2: palladium 10 on activated carbon; hydrogen / ethyl acetate / 12 h / 20 °C / |Inert atmosphere 3: thionyl chloride / dichloromethane / 12 h / |Reflux View Scheme
参考文献
Baek, Dong Jae; MacRitchie, Neil; Anthony, Nahoum G.; MacKay, Simon P.; Pyne, Susan; Pyne, Nigel J.; Bittman, Robert
Journal of Medicinal Chemistry, 2013 , vol. 56, # 22 p. 9310 - 9327
56798-08-4
+
629-05-0
1-辛炔
+
75-24-1
→
反应条件
4588-18-5
反应条件
1: anhydrous 1-octyne; trimethylaluminum With zirconocene dichloride in dichloromethane T=23°C; 6 h; 2: With indium(III) chloride in tetrahydrofuran; dichloromethane T=0°C; 0.5 h; 3: 1-bromo-2-iodoethylene With trifuran-2-yl-phosphane; Cl2Pd[bis(2-diphenylphosphinophenyl)ether]; diisobutylaluminium hydride in tetrahydrofuran; hexane; dichloromethane T=0°C; 4 h;
参考文献
Qian, Mingxing; Huang, Zhihong; Negishi, Ei-Ichi
Organic Letters, 2004 , vol. 6, # 10 p. 1531 - 1534
629-05-0
1-辛炔
+
676-58-4
→
反应条件
4588-18-5
+
41231-86-1
反应条件
copper(I) bromide; lithium bromide in tetrahydrofuran T=0°C; 40 h; Yields of byproduct given;
参考文献
Westmijze, H.; Kleijn, H.; Meijer, J.; Vermeer, P.
Recueil: Journal of the Royal Netherlands Chemical Society, 1981 , vol. 100, # 3 p. 98 - 102
629-05-0
1-辛炔
+
676-58-4
→
反应条件
4588-18-5
反应条件
copper(I) bromide in tetrahydrofuran T=0°C; 40 h; Yield given. Yields of byproduct given;
参考文献
Westmijze, H.; Kleijn, H.; Meijer, J.; Vermeer, P.
Recueil: Journal of the Royal Netherlands Chemical Society, 1981 , vol. 100, # 3 p. 98 - 102
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