反应条件
1: 1) n-BuLi / 1a) diglyme, RT, 1b) 50 deg C, 2) diglyme, 110 deg C
2: 1) dicyclohexylborane / 1) THF, RT, 2 h, 2) MeOH, 4 h, reflux
3: 1) dicyclohexylborane, 2) NaOH, H2O2 / 1a) THF, RT, 1b) diglyme, reflux
4: 55 percent / trialkylammonium chloride, Adogen 464, AcOH, KMnO4 / CH2Cl2; H2O / Heating
View Scheme
参考文献
Brown, Herbert C.; Iyer, Ramakrishnan R.; Bhat, Narayan G.; Racherla, Uday S.; Brown, Charles A.
Tetrahedron, 1992 , vol. 48, # 42 p. 9187 - 9194
