(R)-(-)-1,3-丁二醇合成路线 (共 27 条)
反应条件
hydrogenchloride in methanol 14 h; Ambient temperature;
参考文献
Harada, Toshiro; Kurokawa, Hideaki; Oku, Akira
Tetrahedron Letters, 1987 , vol. 28, # 41 p. 4843 - 4846
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
Sharma, Gangavaram V. M.; Reddy, Post Sai
European Journal of Organic Chemistry, 2012 , # 12 p. 2414 - 2421
反应条件
lithium aluminium tetrahydride in 1,4-dioxane T=80°C; 3 h; Heating;
参考文献
Murakami, Shigeki; Harada, Tadao; Tai, Akira
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 5 p. 1356 - 1360
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C; 6 h; Inert atmosphere;
参考文献
Arkivoc, , vol. 2013, # 4 p. 164 - 170
反应条件
phosphate buffer; pKK-CPA1 in water T=30°C; Isomerization; pH=6.5; 24 h;
参考文献
Bioscience, Biotechnology and Biochemistry, , vol. 63, # 6 p. 1051 - 1055
反应条件
toluene-4-sulfonic acid in methanol Ambient temperature; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 57, # 5 p. 1412 - 1421
反应条件
sodium hydroxide in methanol Heating; Yield given;
参考文献
Tetrahedron Letters, , vol. 28, # 41 p. 4847 - 4848
反应条件
dimercaptoethane; camphor-10-sulfonic acid in dichloromethane Ambient temperature; Yield given;
参考文献
Tetrahedron Letters, , vol. 38, # 37 p. 6607 - 6610
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Tetrahedron Letters, , vol. 40, # 21 p. 4093 - 4096
反应条件
potassium carbonate; (R,R)-iPrDuPhos 1) CH2Cl2, 2 h, 20-25 deg C, 2) MeOH, 4 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 33, # 16 p. 2099 - 2102