2,7-二硝基-5,10-二氧代-4,9-二氧杂芘合成路线 （共 3 条）
反应条件
sulfuric acid; bromine; nitric acid
T=55 - 80°C; 4.5 h;
参考文献
Andrievskii; Gorelik; Linko; Grachev
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 10 p. 1474 - 1481
Zhurnal Organicheskoi Khimii, 2013 , vol. 49, # 10 p. 1496 - 1502,7
反应条件
1: bromine; sulfuric acid; nitric acid / 3 h / 50 - 65 °C
2: N,N-dimethyl-formamide / 3 h / |Reflux
View Scheme
参考文献
Andrievskii; Gorelik; Linko; Grachev
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 10 p. 1474 - 1481
Zhurnal Organicheskoi Khimii, 2013 , vol. 49, # 10 p. 1496 - 1502,7
反应条件
1: bromine; sulfuric acid; nitric acid / 4.5 h / 55 - 80 °C
2: N,N-dimethyl-formamide / 3 h / |Reflux
View Scheme
参考文献
Andrievskii; Gorelik; Linko; Grachev
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 10 p. 1474 - 1481
Zhurnal Organicheskoi Khimii, 2013 , vol. 49, # 10 p. 1496 - 1502,7
