4,4'-二甲基二苯基碘鎓合成路线 (共 21 条)
反应条件
zinc; bis(acetylacetonato) palladium in tetrahydrofuran 0.05 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 1165 - 1166
反应条件
zinc; palladium diacetate in acetone 1 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 1201 - 1202
反应条件
palladium dichloride in water Suzuki coupling; 0.00555556 h; microwave irradiation;
参考文献
Yan, Jie; Zhou, Zhongshi; Zhu, Min
Synthetic Communications, 2006 , vol. 36, # 11 p. 1495 - 1502
反应条件
(NH4)2S2O8 in sulfuric acid; toluene
参考文献
Nippon Petrochemicals Co., Ltd.
Patent: US4659840 A1, 1987 ;
反应条件
1: With Chretien's reagent; sulfuric acid; acetic anhydride
T=20°C; 20 h;
2: With potassium bromide in water
参考文献
Kraszkiewicz, Lukasz; Skulski, Lech
Synthesis, 2008 , # 15 art. no. Z06808SS, p. 2373 - 2380
反应条件
KIO3; sulfuric acid; acetic anhydride; acetic acid
Behandeln einer Loesung des Reaktionsprodukts in Wasser mit Natriumbromid;
参考文献
Beringer et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 2705,2707
Journal of the American Chemical Society, 1959 , vol. 81, p. 342,346
反应条件
(i) nBuLi, (ii) /BRN= 1936384/; Multistep reaction;
参考文献
Beringer,F.M. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 2948 - 2952
反应条件
sodium hydroxide
Heating;
参考文献
Crowder,J.R. et al.
Journal of the Chemical Society, 1963 , p. 4578 - 4585
反应条件
indium(III) chloride; sodium tetrahydroborate in acetonitrile
T=-15 - 20°C; 15 h;
参考文献
Xue, Zhao; Yang, Deyu; Wang, Chunyan
Journal of Organometallic Chemistry, 2006 , vol. 691, # 1-2 p. 247 - 250
反应条件
sodium hydride; 1-n-butyl-3-methylimidazolium tetrafluoroborate
T=40°C;
参考文献
Wang, Feng-Yan; Chen, Zhen-Chu; Zheng, Qin-Guo
Journal of Chemical Research, 2004 , # 3 p. 206 - 207