(E)-5-十二烯-1-醇合成路线 （共 5 条）
反应条件
lithium aluminium tetrahydride in diethyl ether
3 h; Heating;
参考文献
Verba, G. G.; Bukulova, L. M.; Abduvakhabov, A. A.; Kamaev, F. G.
Chemistry of Natural Compounds, 1991 , vol. 27, # 1 p. 113 - 116
Khimiya Prirodnykh Soedinenii, 1991 , # 1 p. 129 - 132
反应条件
1: 65 percent / LiAlH4 / diethyl ether / 3 h / Heating
2: 67 percent / PBr3, pyridine / diethyl ether / 1. -5 deg C to 0 deg C, 1 day, 2. reflux, 2 h
4: 72 percent / LiAlH4 / diethyl ether / 3 h / Heating
View Scheme
参考文献
Verba, G. G.; Bukulova, L. M.; Abduvakhabov, A. A.; Kamaev, F. G.
Chemistry of Natural Compounds, 1991 , vol. 27, # 1 p. 113 - 116
Khimiya Prirodnykh Soedinenii, 1991 , # 1 p. 129 - 132
反应条件
1: 68 percent / piperidine / xylene / 4 h / Heating
2: 65 percent / LiAlH4 / diethyl ether / 3 h / Heating
3: 67 percent / PBr3, pyridine / diethyl ether / 1. -5 deg C to 0 deg C, 1 day, 2. reflux, 2 h
5: 72 percent / LiAlH4 / diethyl ether / 3 h / Heating
View Scheme
参考文献
Verba, G. G.; Bukulova, L. M.; Abduvakhabov, A. A.; Kamaev, F. G.
Chemistry of Natural Compounds, 1991 , vol. 27, # 1 p. 113 - 116
Khimiya Prirodnykh Soedinenii, 1991 , # 1 p. 129 - 132
反应条件
1: 67 percent / PBr3, pyridine / diethyl ether / 1. -5 deg C to 0 deg C, 1 day, 2. reflux, 2 h
3: 72 percent / LiAlH4 / diethyl ether / 3 h / Heating
View Scheme
参考文献
Verba, G. G.; Bukulova, L. M.; Abduvakhabov, A. A.; Kamaev, F. G.
Chemistry of Natural Compounds, 1991 , vol. 27, # 1 p. 113 - 116
Khimiya Prirodnykh Soedinenii, 1991 , # 1 p. 129 - 132
反应条件
2: 72 percent / LiAlH4 / diethyl ether / 3 h / Heating
View Scheme
参考文献
Verba, G. G.; Bukulova, L. M.; Abduvakhabov, A. A.; Kamaev, F. G.
Chemistry of Natural Compounds, 1991 , vol. 27, # 1 p. 113 - 116
Khimiya Prirodnykh Soedinenii, 1991 , # 1 p. 129 - 132
