4-苯氧基苯甲酰基甲酸乙酯合成路线 (共 3 条)
反应条件
aluminium trichloride in dichloromethane
T=0°C; Friedel-Crafts acylation; 2 h;
参考文献
Imoto, Hiroshi; Imamiya, Eikoh; Momose, Yu; Sugiyama, Yasuo; Kimura, Hiroyuki; Sohda, Takashi
Chemical and Pharmaceutical Bulletin, 2002 , vol. 50, # 10 p. 1349 - 1357
反应条件
AlCl3 in dichloromethane
参考文献
Ciba Specialty Chemicals Corp.
Patent: US6258954 B1, 2001 ;
反应条件
1: 4-bromophenyl phenyl ether With magnesium in tetrahydrofuran
T=20°C; 1 h;
2: oxalic acid diethyl ester in tetrahydrofuran
T=-78 - -10°C; 1 h;
参考文献
Shirai, Tomohiko; Ito, Hajime; Yamamoto, Yasunori
Angewandte Chemie - International Edition, 2014 , vol. 53, # 10 p. 2658 - 2661
Angew. Chem., 2014 , vol. 126, # 10 p. 2696 - 2699,4