chromium sulphate in N,N-dimethyl-formamide
T=20°C; 72 h;
参考文献
Davies, Stephen G.; Haggitt, Jane R.; Ichihara, Osamu; Kelly, Richard J.; Leech, Michael A.; Mortimer, Anne J. Price; Roberts, Paul M.; Smith, Andrew D.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 18 p. 2630 - 2649
1: 77 percent / CrO3; H2SO4 / acetone / 2.5 h / 20 °C
2: 64 percent / aq. CrSO4 / dimethylformamide / 72 h / 20 °C
View Scheme
参考文献
Davies, Stephen G.; Haggitt, Jane R.; Ichihara, Osamu; Kelly, Richard J.; Leech, Michael A.; Mortimer, Anne J. Price; Roberts, Paul M.; Smith, Andrew D.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 18 p. 2630 - 2649
1: 90 percent / PTSA / methanol / 2 h / 50 - 60 °C
2: 77 percent / CrO3; H2SO4 / acetone / 2.5 h / 20 °C
3: 64 percent / aq. CrSO4 / dimethylformamide / 72 h / 20 °C
View Scheme
参考文献
Davies, Stephen G.; Haggitt, Jane R.; Ichihara, Osamu; Kelly, Richard J.; Leech, Michael A.; Mortimer, Anne J. Price; Roberts, Paul M.; Smith, Andrew D.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 18 p. 2630 - 2649