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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
黄腐酚
合成路线
（共 12 条）
1314539-28-0
→
反应条件
62949-76-2
黄腐酚
反应条件
carbon tetrabromide in isopropyl alcohol 5 h; Reflux;
参考文献
Sugamoto, Kazuhiro; Matsusita, Yoh-Ichi; Matsui, Kana; Kurogi, Chiaki; Matsui, Takanao
Tetrahedron, 2011 , vol. 67, # 29 p. 5346 - 5359
1544322-63-5
→
反应条件
62949-76-2
黄腐酚
反应条件
hydrogenchloride; methanol in water 6 h; Inert atmosphere;
参考文献
Wang, Haomeng; Yan, Zhihong; Lei, Yanan; Sheng, Kai; Yao, Qingwei; Lu, Kui; Yu, Peng
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 897 - 899
1229515-77-8
→
反应条件
62949-76-2
黄腐酚
反应条件
hydrogenchloride in methanol T=20°C; 10 h; Inert atmosphere;
参考文献
Jung, Doo Hwan; Lee, Yong Rok; Kim, Sung Hong
Helvetica Chimica Acta, 2010 , vol. 93, # 4 p. 635 - 647
89-84-9
2,4-二羟基苯乙酮
→
反应条件
62949-76-2
黄腐酚
反应条件
1: potassium carbonate / acetone / 3 h / 0 °C 2: potassium carbonate / acetone / 24 h / Reflux 3: sodium hydroxide / ethanol / 72 h / 0 - 20 °C 4: montmorillonite K10 / dichloromethane / 2 h / 0 °C 5: carbon tetrabromide / isopropyl alcohol / 5 h / Reflux View Scheme
参考文献
Sugamoto, Kazuhiro; Matsusita, Yoh-Ichi; Matsui, Kana; Kurogi, Chiaki; Matsui, Takanao
Tetrahedron, 2011 , vol. 67, # 29 p. 5346 - 5359
1314539-21-3
→
反应条件
62949-76-2
黄腐酚
反应条件
1: sodium hydroxide / ethanol / 72 h / 0 - 20 °C 2: montmorillonite K10 / dichloromethane / 2 h / 0 °C 3: carbon tetrabromide / isopropyl alcohol / 5 h / Reflux View Scheme
参考文献
Sugamoto, Kazuhiro; Matsusita, Yoh-Ichi; Matsui, Kana; Kurogi, Chiaki; Matsui, Takanao
Tetrahedron, 2011 , vol. 67, # 29 p. 5346 - 5359
1314539-25-7
→
反应条件
62949-76-2
黄腐酚
反应条件
1: montmorillonite K10 / dichloromethane / 2 h / 0 °C 2: carbon tetrabromide / isopropyl alcohol / 5 h / Reflux View Scheme
参考文献
Sugamoto, Kazuhiro; Matsusita, Yoh-Ichi; Matsui, Kana; Kurogi, Chiaki; Matsui, Takanao
Tetrahedron, 2011 , vol. 67, # 29 p. 5346 - 5359
6515-21-5
→
反应条件
62949-76-2
黄腐酚
反应条件
1: sodium hydroxide / ethanol / 72 h / 0 - 20 °C 2: montmorillonite K10 / dichloromethane / 2 h / 0 °C 3: carbon tetrabromide / isopropyl alcohol / 5 h / Reflux View Scheme
参考文献
Sugamoto, Kazuhiro; Matsusita, Yoh-Ichi; Matsui, Kana; Kurogi, Chiaki; Matsui, Takanao
Tetrahedron, 2011 , vol. 67, # 29 p. 5346 - 5359
65490-08-6
→
反应条件
62949-76-2
黄腐酚
反应条件
1: potassium carbonate / acetone / 24 h / Reflux 2: sodium hydroxide / ethanol / 72 h / 0 - 20 °C 3: montmorillonite K10 / dichloromethane / 2 h / 0 °C 4: carbon tetrabromide / isopropyl alcohol / 5 h / Reflux View Scheme
参考文献
Sugamoto, Kazuhiro; Matsusita, Yoh-Ichi; Matsui, Kana; Kurogi, Chiaki; Matsui, Takanao
Tetrahedron, 2011 , vol. 67, # 29 p. 5346 - 5359
123-08-0
对羟基苯甲醛
→
反应条件
62949-76-2
黄腐酚
反应条件
1: potassium carbonate / acetone / 2 h / 20 °C 2: sodium hydroxide / ethanol / 72 h / 0 - 20 °C 3: montmorillonite K10 / dichloromethane / 2 h / 0 °C 4: carbon tetrabromide / isopropyl alcohol / 5 h / Reflux View Scheme
参考文献
Sugamoto, Kazuhiro; Matsusita, Yoh-Ichi; Matsui, Kana; Kurogi, Chiaki; Matsui, Takanao
Tetrahedron, 2011 , vol. 67, # 29 p. 5346 - 5359
71243-12-4
→
反应条件
62949-76-2
黄腐酚
反应条件
1: sodium hydride / dichloromethane / 2 h / 0 °C / |Inert atmosphere 2: potassium hydroxide / ethanol; water / 12 h / 0 - 20 °C / |Inert atmosphere 3: caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 2 h / 70 °C / |Inert atmosphere; |Microwave irradiation 4: hydrogenchloride; methanol / water / 6 h / |Inert atmosphere View Scheme
参考文献
Wang, Haomeng; Yan, Zhihong; Lei, Yanan; Sheng, Kai; Yao, Qingwei; Lu, Kui; Yu, Peng
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 897 - 899
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