1,2-环己烷二羧酸二丁酯合成路线 （共 3 条）
反应条件
nickel
T=150°C; P=76000 Torr; Hydrogenation;
参考文献
Matsuda; Kikkawa
Kogyo Kagaku Zasshi, 1956 , vol. 59, p. 895,897
Technology Reports of the Osaka University, 1957 , vol. 7, p. 199,203
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Matsuda; Kikkawa
Technology Reports of the Osaka University, 1957 , vol. 7, p. 199,201, 202
Kogyo Kagaku Zasshi, 1956 , vol. 59, p. 895,896
Chem.Abstr., 1958 , p. 10001
反应条件
1: 4,5,6,7,3a,7a-hexahydroisobenzofuran-1,3-dione; butan-1-ol T=130°C; 1 h;
2: 8-methyl-1-nonanol; butan-1-ol With tin oxide
T=220°C; P=150.015 Torr; 10 h; Dean-Stark trap; Product distribution / selectivity;
参考文献
New Japan Chemical, Co., Ltd.
Patent: US2005/38283 A1, 2005 ;
Location in patent: Page/Page column 42 ;
反应条件
sodium n-butanolate
Entfernen des entstehenden Methanols;
参考文献
McKusick
Journal of the American Chemical Society, 1948 , vol. 70, p. 1982
