3-乙氧基-6-甲基-2-环己烯-1-酮合成路线 (共 2 条)
反应条件
1: 3-ethoxy-2-cyclohexen-1-one With lithium diisopropyl amide in tetrahydrofuran; hexane
T=-78°C; 1 h;
2: methyl iodide in tetrahydrofuran; hexane
T=-78 - 25°C; 1 h;
参考文献
Trost, Barry M.; Bream, Robert N.; Xu, Jiayi
Angewandte Chemie - International Edition, 2006 , vol. 45, # 19 p. 3109 - 3112
反应条件
1: 3-ethoxy-6-methyl-2-cyclohexen-1-one With lithium diisopropyl amide in tetrahydrofuran; hexane
T=-78°C; 2 h;
2: methyl iodide in tetrahydrofuran; hexane
T=-78 - 20°C; Further stages.;
参考文献
Foote, Kevin M; Hayes, Christopher J; John, Matthew P; Pattenden, Gerald
Organic and biomolecular chemistry, 2003 , vol. 1, # 22 p. 3917 - 3948