4-溴-2,6-双羟基甲基苯酚合成路线 (共 9 条)
反应条件
sodium hydroxide T=50°C; 120 h;
参考文献
No, Kwanghyun; Kwon, Kyoung Mee
Synthesis, 1996 , # 11 p. 1293 - 1295
反应条件
Zn(BH4)2(bpy) in acetonitrile T=20°C; 0.0333333 h;
参考文献
Zeynizadeh, Behzad; Yahyaei, Saiedeh
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2004 , vol. 59, # 6 p. 704 - 710
反应条件
sodium hydroxide; formaldehyd in water; acetic acid; aluminium
参考文献
Alcon, Inc.
Patent: US2011/3910 A1, 2011 ;
反应条件
manganese(IV) oxide in chloroform 8 h; Heating;
参考文献
Xie; Zhang; Yan; Yuan
Synthetic Communications, 1994 , vol. 24, # 1 p. 53 - 58
参考文献
Fisher, Thomas H.; Chao, Ping; Upton, G. Cindy; Day, Anthony J.
Magnetic Resonance in Chemistry, 1995 , vol. 33, # 9 p. 717 - 723
反应条件
toluene-4-sulfonic acid in benzene
参考文献
No, Kwanghyun; Kwon, Kyoung Mee
Synthesis, 1996 , # 11 p. 1293 - 1295
参考文献
Sharghi; Nasseri; Niknam
Journal of Organic Chemistry, 2001 , vol. 66, # 22 p. 7287 - 7293
反应条件
1: toluene-4-sulfonic acid
2: palladium/charcoal; aq.-ethanolic NaOH / Hydrogenation
View Scheme
参考文献
Davis et al.
Journal of Applied Chemistry, 1953 , vol. 3, p. 312,316
反应条件
1: K2CO3 / dimethylformamide / 24 h / 0 °C
2: 21.0 g / SOCl2 / dimethylformamide; CH2Cl2 / 17 h / 20 °C
View Scheme
参考文献
Tsubaki, Kazunori; Otsubo, Tadamune; Morimoto, Tatsuya; Maruoka, Hiromi; Furukawa, Mika; Momose, Yashima; Shang, Muhong; Fuji, Kaoru
Journal of Organic Chemistry, 2002 , vol. 67, # 23 p. 8151 - 8156