S-[2-(氯甲酰基)苯基]硫代乙酸酯合成路线 （共 5 条）
反应条件
1.1: magnesium / ethanol; tetrachloromethane; diethyl ether / 3.5 h / |Reflux 1.2: 0.5 h / 20 °C 2.1: hydrogenchloride / ethanol / 3 h / |Reflux 3.1: hydrogenchloride / ethanol; water / 2 h / |Reflux View Scheme
参考文献
Arjunan; Santhanam; Sakiladevi; Marchewka; Mohan
Journal of Molecular Structure, 2013 , vol. 1037, p. 305 - 316
反应条件
thionyl chloride
T=50 - 60°C; 3 h;
参考文献
Bhatt, M. Vivekananda; El Ashry, Shaker H.; Somayaji, Vishwanatha
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 6 p. 473 - 486
反应条件
1: acetic acid
2: SOCl2 / 3 h / 50 - 60 °C
View Scheme
参考文献
Bhatt, M. Vivekananda; El Ashry, Shaker H.; Somayaji, Vishwanatha
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 6 p. 473 - 486
反应条件
1: 85 percent / hydriodic acid, hypophosphorous acid, conc. hydrochloric acid / 3 h / Heating
2: acetic acid
3: SOCl2 / 3 h / 50 - 60 °C
View Scheme
参考文献
Bhatt, M. Vivekananda; El Ashry, Shaker H.; Somayaji, Vishwanatha
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 6 p. 473 - 486
反应条件
1.1: NaH / diethyl ether / 0.5 h / 20 °C
1.2: 8.1 g / toluene; diethyl ether / 0.5 h / 20 °C
2.1: 74 percent / 3N HCl / ethanol / 3 h / Heating
3.1: 84 percent / HCl / H2O; ethanol / 3 h / Heating
View Scheme
参考文献
Jung, Jae-Chul; Kim, Ju-Cheun; Park, Oee-Sook
Synthetic Communications, 2000 , vol. 30, # 7 p. 1193 - 1203
