1-(4-甲氧基苯基)乙胺合成路线 （共 45 条）
反应条件
H2; Pd on carbon in methanol
参考文献
US5438118 A1, ;
US 5438118 A
反应条件
1: With borane; (S)-(-)-diphenylvalinol in tetrahydrofuran T=20°C; 20 h; 2: With hydrogenchloride in tetrahydrofuran T=20°C; 30 h; Further stages.;
参考文献
Laczkowski, Krzysztof Z.; Pakulski, Marcin M.; Krzeminski, Marek P.; Jaisankar, Parasuraman; Zaidlewicz, Marek
Tetrahedron Asymmetry, 2008 , vol. 19, # 7 p. 788 - 795
反应条件
1: With [((R)-tol-binap)RuCl2(DMF)x]; ammonia; ammonium formate in methanol T=85°C; Leuckart-Wallach reaction; 24 h; 2: With hydrogenchloride in ethanol 1 h; Heating; Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 42, # 44 p. 5472 - 5474
反应条件
6-(1,2:3,4-di-O-isopropylidene-α-D-galactopyranosyl) hydrogen phthalate in isopropyl alcohol Heating;
参考文献
Mereyala, Hari Babu; Fatima, Liyakat; Pola, Pallavi
Tetrahedron Asymmetry, 2004 , vol. 15, # 4 p. 585 - 587
反应条件
1: With trichlorosilane in chloroform T=-10°C; 24 h; 2: With hydrogen; palladium on activated charcoal in methanol T=20°C; 2 h; Further stages. Title compound not separated from byproducts.;
参考文献
Tetrahedron Letters, , vol. 48, # 45 p. 7934 - 7937
反应条件
1: With borane-THF; (S)-proline (R)-1,1'-bi(2-naphthyl)dioxyboryl ester in tetrahydrofuran T=0 - 5°C; 48 h; 2: With hydrogenchloride in tetrahydrofuran Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 71, # 10 p. 3998 - 4001
反应条件
1.1: 85 percent / hydroxylamine hydrochloride; K2CO3 / ethanol / 24 h / Heating 2.1: NaH / dimethylformamide / 2 h / 0 °C 2.2: 80 percent / dimethylformamide / 4 h / 0 - 20 °C 3.1: BH3*THF; (S)-proline (R)-1,1'-bi(2-naphthyl)dioxyboryl ester / tetrahydrofuran / 48 h / 0 - 5 °C 3.2: aq. HCl / tetrahydrofuran View Scheme
参考文献
Journal of Organic Chemistry, , vol. 71, # 10 p. 3998 - 4001
反应条件
ueber das saure Tartrat; Trennung von dem Salz der rechtsdrehenden Form durch Krystallisation aus Alkohol, in dem sich das Salz der linksdrehenden Form leichter loest;
参考文献
Gazzetta Chimica Italiana, , vol. 42 I, p. 285
反应条件
hydroxylamine-o-sulphonic acid in tetrahydrofuran Substitution; 10 h;
参考文献
Chemistry - A European Journal, , vol. 6, # 10 p. 1840 - 1846
反应条件
Candida antartica lipase (N-435) in toluene T=40°C;
参考文献
Tetrahedron Letters, , vol. 43, # 26 p. 4699 - 4702
