(9ci)-1H-苯并咪唑-1-胺合成路线 （共 12 条）
反应条件
sulfur a) from 165 to 170 deg C, 15 min, b) from 295 to 300 deg C, 1 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 28, # 11.1 p. 1880 - 1884
Zhurnal Organicheskoi Khimii, , vol. 28, # 11 p. 2328 - 2333
反应条件
18-crown-6 ether in acetonitrile T=20°C; Deamination; 2 h;
参考文献
Itoh, Takashi; Miyazaki, Michiko; Maeta, Hiromi; Matsuya, Yuji; Nagata, Kazuhiro; Ohsawa, Akio
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 8 p. 1983 - 1989
反应条件
lead(IV) acetate; CaO in dichloromethane T=20 - 25°C; 1 h;
参考文献
Pozharskii, A. F.; Nanavyan, I. M.; Kuz'menko, V. V.; Chernyshev, A. I.; Orlov, Yu. V.; Klyuev, N. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 11 p. 1241 - 1253
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 11 p. 1486 - 1499
反应条件
in dichloromethane T=20°C; 1 h; other 1-aminobenzimidazole, other time; Product distribution;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 25, # 11 p. 1241 - 1253
Khimiya Geterotsiklicheskikh Soedinenii, , # 11 p. 1486 - 1499
反应条件
ammonia; KNH2 1.) -78 deg C, 10 min, 2.) -78 deg C, 30 min; Multistep reaction. Yields of byproduct given;
参考文献
Kuz'menko, V. V.; Filatova, I. A.; Pozharskii, A. F.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1992 , vol. 28, # 9 p. 1009 - 1014
Khimiya Geterotsiklicheskikh Soedinenii, 1992 , # 9 p. 1196 - 1201
反应条件
potassium hydroxide; sodium hydrogencarbonate; hydroxylamine-o-sulphonic acid in water
T=40 - 45°C; 0.0833333 h;
参考文献
Pozharskii, A.F.; Kuz'menko, V.V.; Bumber, A.A.; Petrov, E.S.; Terekhova, M.I.; et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 2 p. 180 - 186
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 2 p. 221 - 227
反应条件
hydrogenchloride
0.0166667 h; Heating;
参考文献
Gelvin, Christopher R.; Turnbull, Kenneth
Helvetica Chimica Acta, 1992 , vol. 75, # 6 p. 1931 - 1943
反应条件
hydrogenchloride
0.0166667 h; Heating;
参考文献
Gelvin, Christopher R.; Turnbull, Kenneth
Helvetica Chimica Acta, 1992 , vol. 75, # 6 p. 1931 - 1943
反应条件
1: 72 percent / CHCl3 / 1 h / 55 - 60 °C
2: 56 percent / conc. HCl / 8.5 h / Heating
View Scheme
参考文献
Vinogradova, O. V.; Kryshtalyuk, O. V.; Rudnev, M. I.; Pozharskii, A. F.; Kuz'menko, V. V.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1994 , vol. 30, # 10 p. 1182 - 1186
Khimiya Geterotsiklicheskikh Soedinenii, 1994 , # 10 p. 1364 - 1368
反应条件
meta-nitrobenzenesulfonic acid
参考文献
Abramovitch; Schofield
Journal of the Chemical Society, 1955 , p. 2326,2331
