反应条件
4-(N,N-dimethlyamino)pyridine; 2,4,6-trichlorobenzoyl chloride; titanium tetrachloride; triethylamine 1.) THF, toluene, reflux, 6 h, 2.) CH2Cl2, 0 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Haynes, Richard K.; Lam, William W.-L.; Yeung, Lam-Lung; Williams, Ian D.; Ridley, Andrew C.; Starling, Scott M.; Vonwiller, Simone C.; Hambley, Trevor W.; Lelandais, Patrick
Journal of Organic Chemistry, 1997 , vol. 62, # 14 p. 4552 - 4553