[二(甲硫基)甲基]膦酸二乙酯合成路线 (共 14 条)
反应条件
triethyl phosphite; phosphorus trichoride
Yield given. Multistep reaction;
参考文献
Gross, Hans; Keitel, Iris; Costisella, Burkhard; Mikolajczyk, Marian; Midura, Wanda
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 257 - 262
参考文献
Mikolajczyk,M. et al.
Journal of Organic Chemistry, 1979 , vol. 44, p. 2967 - 2972
参考文献
Mlotkowska,B. et al.
Journal fuer Praktische Chemie (Leipzig), 1977 , vol. 319, p. 17 - 22
反应条件
1: 85 percent / n-Bu3SnH, AIBN / toluene / 1 h / Heating
2: 80 percent / H2O2 / methanol / 30 h / 25 °C
View Scheme
参考文献
Balczewski,Piotr
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 104, # 14 p. 113 - 122