反应条件
in tetrahydrofuran byproducts: NaI; 2,2-diiodopropane was added all at once to Na(CpCo(CO))2 in THF under N2, 15 min; NaI was pptd. with hexane, mixture was filtered, evapd., chromy., solvent from the third purple fraction was evapd., recrystn. from hexane; elem. anal.;
参考文献
Journal of the American Chemical Society, , vol. 105, # 3 p. 464 - 475
