1-溴-2,2-二甲基丙烷合成路线 （共 70 条）
反应条件
1: toluene / 24 h / 90 °C 2: 30 percent Spectr. / t-BuOK / toluene / 0.33 h / 30 °C 3: 12 percent Chromat. / tetrahydrofuran / 1 h / 0 °C View Scheme
参考文献
Bandmann, Heinz; Bartik, Tamas; Bauckloh, Sylvia; Behler, Ansgar; Brille, Frank; et al.
Zeitschrift fuer Chemie (Stuttgart, Germany), 1990 , vol. 30, # 6 p. 193 - 204
反应条件
tetra-n-butylammonium tetrafluoroborate; superoxide ion in N,N-dimethyl-formamide T=25°C; Rate constant;
参考文献
Daasbjerg, Kim; Lund, Henning
Acta Chemica Scandinavica, 1993 , vol. 47, # 6 p. 597 - 604
反应条件
tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide T=25°C; Rate constant;
参考文献
Daasbjerg, Kim; Lund, Henning
Acta Chemica Scandinavica, 1993 , vol. 47, # 6 p. 597 - 604
反应条件
chloride in gas ΔH0Rx; Thermodynamic data;
参考文献
DePuy, Charles H.; Gronert, Scott; Mullin, Amy; Bierbaum, Veronica M.
Journal of the American Chemical Society, 1990 , vol. 112, # 24 p. 8650 - 8655
反应条件
Et4NN3 in N,N-dimethyl-formamide T=80°C; 10 h;
参考文献
Ponomarchuk, M. P.; Sologub, L. S.; Kasukhin, L. F.; Kukhar', V. P.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 8 p. 1725 - 1730,1532 - 1536
反应条件
1: rac-1,2-dimethyl-1,2,2-triphenyl-1-(N-piperidinomethyl)disilane With lithium in tetrahydrofuran T=0°C; 6 h; Inert atmosphere; 2: 1-bromo-2,2-dimethylpropane in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
European Journal of Inorganic Chemistry, , # 9 p. 1454 - 1465
反应条件
in acetone T=63°C; 3 h; Inert atmosphere;
参考文献
Rojas, Giovanni; Inci, Bora; Wei, Yuying; Wagener, Kenneth B.
Journal of the American Chemical Society, 2009 , vol. 131, # 47 p. 17376 - 17386
参考文献
Kobler,H. et al.
Justus Liebigs Annalen der Chemie, 1978 , p. 1946 - 1962
反应条件
fluorine 2 h; Irradiationvar. F/hydrocarbon mole ratio, without irradiation; Product distribution;
参考文献
Adcock, James L.; Evans, William D.; Heller-Grossman, Lilly
Journal of Organic Chemistry, 1983 , vol. 48, # 25 p. 4953 - 4957
反应条件
tetra-n-butylammonium tetrafluoroborate in N,N-dimethyl-formamide T=25°C; Rate constant;
参考文献
Daasbjerg, Kim; Lund, Henning
Acta Chemica Scandinavica, 1993 , vol. 47, # 6 p. 597 - 604
