Curtin; Gerber
Journal of the American Chemical Society, 1952 , vol. 74, p. 4052,4055
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Shapiro et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3725,3726
hydrogen in benzene-d6 High Pressure; NMR tube charged with (C5Me5)2ScNHCH2CMe3 and C6D6, cooled to 77 K, t-BuCN condensed in, 700 torr of H2 introduced, sealed, reacted at 25°C and 4 atm of H2 for 17 h, heated to 80°C for further 24 h; not isolated; detected by NMR;
参考文献
Bercaw, John E.; Davies, David L.; Wolczanski, Peter T.
Organometallics, 1986 , vol. 5, p. 443 - 450
1: 2-bromo-pyridine With n-butyllithium in diethyl ether T=-78°C; 1.5 h; Inert atmosphere; 2: 2,2-dimethyl-1-propanenitrile in diethyl ether T=-78 - 20°C; Inert atmosphere;
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Diaz-Valenzuela, M. Belen; Phillips, Scott D.; France, Marcia B.; Gunn, Mary E.; Clarke, Matthew L.
Chemistry - A European Journal, 2009 , vol. 15, # 5 p. 1227 - 1232