反应条件
sodium hydroxide; Ipc2B(OMe); boron trifluoride diethyl etherate; dihydrogen peroxide; tert.-butyl lithium 1.) THF, pentane, ether, 0 deg C, 1 h; 0 deg C, 10 min, 2.) 0 deg C, 3. ) ether, -100 deg C, 3 h, 4.) reflux, 1 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brown, Herbert C.; Khire, Uday R.; Narla, Gowriswari
Journal of Organic Chemistry, 1995 , vol. 60, # 25 p. 8130 - 8131
