2,2,2-三甲基硫代乙酰胺合成路线 （共 4 条）
反应条件
P2S5/alumina in tetrahydrofuran T=60°C; 0.333333 h; Microwave irradiation;
参考文献
Orr, David; Tolfrey, Alexandra; Percy, Jonathan M.; Frieman, Joanna; Harrison, Zoe A.; Campbell-Crawford, Matthew; Patel, Vipulkumar K.
Chemistry - A European Journal, 2013 , vol. 19, # 29 p. 9655 - 9662
反应条件
1: With CaH2; ethanethiolic acid T=80°C; 1 h; 2: With water in ethyl acetate T=20°C;
参考文献
Mahammed; Jayashankara; Premsai Rai; Mohana Raju; Arunachalam
Synlett, 2009 , # 14 p. 2338 - 2340
反应条件
in chloroform-d1 T=55°C; Yield given. Yields of byproduct given;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 26, p. 169 - 184
反应条件
1: 58 percent / H2O2 / acetonitrile / 16 h / 5 °C 2: 45 percent / H2O2, 0.1 N NaOH / H2O / 48 h / 25 °C View Scheme
参考文献
Hillhouse, John H.; Blair, Ian A.; Field, Lamar
Phosphorus and Sulfur and the Related Elements, 1986 , vol. 26, p. 169 - 184
