2-氯-2-氟-1-苯基-1-丙酮合成路线 （共 5 条）
反应条件
chlorine in N,N-dimethyl-formamide
T=100°C; 0.5 h;
参考文献
Kimpe, Norbert De; Verhe, Roland; Buyck, Laurent De; Schamp, Niceas
Journal of Organic Chemistry, 1980 , vol. 45, # 14 p. 2803 - 2813
反应条件
mercury(II) fluoride
T=140 - 160°C;
参考文献
Modarai,B.; Khoshdel,E.
Journal of Organic Chemistry, 1977 , vol. 42, # 22 p. 3527 - 3531
反应条件
1: 60 percent / KF / dimethylformamide / 3 h / 110 °C
2: 82 percent / Cl2 / dimethylformamide / 0.5 h / 100 °C
View Scheme
参考文献
Kimpe, Norbert De; Verhe, Roland; Buyck, Laurent De; Schamp, Niceas
Journal of Organic Chemistry, 1980 , vol. 45, # 14 p. 2803 - 2813
反应条件
1: 100 percent / Br2 / CCl4 / 0.17 h
2: 60 percent / KF / dimethylformamide / 3 h / 110 °C
3: 82 percent / Cl2 / dimethylformamide / 0.5 h / 100 °C
View Scheme
参考文献
Kimpe, Norbert De; Verhe, Roland; Buyck, Laurent De; Schamp, Niceas
Journal of Organic Chemistry, 1980 , vol. 45, # 14 p. 2803 - 2813
反应条件
1: NBS / CCl4 / Irradiation
2: HgF2 / 140 - 160 °C
View Scheme
参考文献
Modarai,B.; Khoshdel,E.
Journal of Organic Chemistry, 1977 , vol. 42, # 22 p. 3527 - 3531
