1-(4-氯苯基)1,3-丁二酮合成路线 （共 27 条）
反应条件
hydrogenchloride Heating;
参考文献
Bulletin de la Societe Chimique de France, , p. 1293 - 1295
反应条件
aluminium trichloride; tetrachloroethane, 1,1,2,2-
参考文献
Chemische Berichte, , vol. 84, p. 607,615
反应条件
1: With diethylamine T=20 - 25°C; 19 - 51 h; Heating / reflux; 2: With hydrogenchloride; water T=20°C; 0.5 h;
参考文献
McArthur, Silvia Gatti; Goetschi, Erwin; Wichmann, Juergen; Woltering, Thomas Johannes
Patent: US2007/232583 A1, 2007 ;
Location in patent: Page/Page column 24; 25; 33 ;
US 20070232583 A1
反应条件
piperidine in ethanol T=70°C; 5 h;
参考文献
Krstic, Vera; Misic-Vukovic, Milica; Radojkovic-Velickovic, Mirjana
Journal of Chemical Research, Miniprint, 1991 , # 4 p. 783 - 792
反应条件
in water T=40°C; 144 h; lipase from Candida cylindracea;
参考文献
Mijin, Dusan Z.; Misic-Vukovic, Milica M.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1995 , vol. 34, # 4 p. 348 - 350
反应条件
in water pH=0.8; 4 h; Reflux; regioselective reaction;
参考文献
Aggarwal, Ranjana; Sumran, Garima; Garg, Neelam; Aggarwal, Ashok
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 7 p. 3038 - 3046
反应条件
thiocarbonohydrazide
参考文献
Alekseev, V. V.; Zelenin, K. N.; Yakimovich, S. I.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 6 p. 868 - 873
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 6 p. 937 - 943
反应条件
hydrazine in methanol T=13°C; Rate constant;
参考文献
Selivanov, S. I.; Golodova, K. G.; Abbasov, Ya. A.; Ershov, B. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 7 p. 1361 - 1364
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 7 p. 1494 - 1497
反应条件
1: 55 percent / EtONa / ethanol 2: 24 percent / ethanol / 1.5 h / Ambient temperature View Scheme
参考文献
Dal Piaz; Ciciani; Giovannoni
Farmaco, 1991 , vol. 46, # 3 p. 435 - 447
反应条件
in tetrahydrofuran
6 h; Reflux;
参考文献
Eakta; Aggarwal, Ranjana; Sumran, Garima
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 2 p. 273 - 281
