4-(3,4-二甲氧基苯基)丁烷-2-酮合成路线 (共 17 条)
参考文献
Nomura
Journal of the Chemical Society, 1917 , vol. 111, p. 771
Full Text Show Details
Lapworth; Pearson; Royle
Journal of the Chemical Society, 1917 , vol. 111, p. 786
参考文献
Nomura
Journal of the Chemical Society, 1917 , vol. 111, p. 771
Full Text Show Details
Lapworth; Pearson; Royle
Journal of the Chemical Society, 1917 , vol. 111, p. 786
参考文献
Journal of the Chemical Society, , vol. 111, p. 771
Journal of the Chemical Society, , vol. 111, p. 786
反应条件
1.1: LDA / tetrahydrofuran / 0.33 h / -78 °C 1.2: tetrahydrofuran / 3 h / -78 - 20 °C 2.1: 74 percent / 1,4-dicyanonaphthalene / acetonitrile; H2O / 4 h / Irradiation View Scheme
参考文献
Pandey; Krishna; Girija; Karthikeyan
Tetrahedron Letters, 1993 , vol. 34, # 41 p. 6631 - 6634
反应条件
palladium 10 on activated carbon; hydrogen in methanol
P=1551.49 Torr; 3 h;
参考文献
Dhuru, Sameer; Bhedi, Dilip; Gophane, Dnyaneshwar; Hirbhagat, Kiran; Nadar, Vijaya; More, Dattatray; Parikh, Sapna; Dalal, Roda; Fonseca, Lyle C.; Kharas, Firuza; Vadnal, Prashant Y.; Vishwakarma, Ram A.; Sivaramakrishnan
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 12 p. 3784 - 3787
反应条件
methanol; formic acid; water; silica gel; palladium dichloride
0.816667 h; Irradiationmicrowave;
参考文献
Sharma, Anuj; Kumar, Vinod; Sinha, Arun K.
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 3 p. 354 - 360
反应条件
potassium carbonate in acetone
Reflux;
参考文献
Sanfilippo, Claudia; Patti, Angela; Dettori, Maria Antonietta; Fabbri, Davide; Delogu, Giovanna
Journal of Molecular Catalysis B: Enzymatic, 2013 , vol. 90, p. 107 - 113
反应条件
DCN in water; acetonitrile
3 h; Irradiation;
参考文献
Pandey; Krishna; Girija; Karthikeyan
Tetrahedron Letters, 1993 , vol. 34, # 41 p. 6631 - 6634
反应条件
1: aq. NaOH
2: 84 percent / H2 / Pd/C / ethanol
View Scheme
参考文献
Pandey, Ganesh; Karthikeyan; Murugan
Journal of Organic Chemistry, 1998 , vol. 63, # 9 p. 2867 - 2872
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
1 h;
参考文献
Batra, Sanjay; Seth, M; Bhaduri, A P
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 1 p. 60 - 62