2-(4-甲氧基苯基)-1-咪唑啉合成路线 (共 16 条)
参考文献
Oxley; Short
Journal of the Chemical Society, 1947 , p. 497,500
反应条件
iodine; potassium carbonate in tert-butyl alcohol
T=70°C; 3 h;
参考文献
Ishihara, Midori; Togo, Hideo
Tetrahedron, 2007 , vol. 63, # 6 p. 1474 - 1480
反应条件
tetraphosphorus decasulfide
0.133333 h; microwave irradiation;
参考文献
Moghadam, Majid; Mohammadpoor-Baltork, Iraj; Mirkhani, Valiollah; Tangestaninejad, Shahram; Abdollahi-Alibeik, Mohammad; Yousefi, Behrooz H.; Kargar, Hadi
Monatshefte fur Chemie, 2007 , vol. 138, # 6 p. 579 - 583
反应条件
1: (4-methoxyphenyl)methanol With iodine; potassium carbonate in tert-butyl alcohol
T=70°C; 8 h;
2: ethylenediamine in tert-butyl alcohol
T=70°C; 2 h;
参考文献
Ishihara, Midori; Togo, Hideo
Tetrahedron, 2007 , vol. 63, # 6 p. 1474 - 1480
反应条件
1,3-bis-(diphenylphosphino)propane; caesium carbonate; palladium dichloride in toluene
16 h; Inert atmosphereReflux;
参考文献
Geden, Joanna V.; Pancholi, Alpa K.; Shipman, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4158 - 4164
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; caesium carbonate in toluene
16 h; Inert atmosphereReflux;
参考文献
Geden, Joanna V.; Pancholi, Alpa K.; Shipman, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4158 - 4164
参考文献
Shi, Zhen; Gu, Huan
Synthetic Communications, 1997 , vol. 27, # 15 p. 2701 - 2707
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; caesium carbonate in toluene
16 h; Inert atmosphereReflux;
参考文献
Geden, Joanna V.; Pancholi, Alpa K.; Shipman, Michael
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4158 - 4164
反应条件
1: tert-butyl hypochlorite / 2-methyl-propan-2-ol / 20 °C
2: tert-butyl hypochlorite; potassium iodide / 2-methyl-propan-2-ol / 10 h / 50 °C
View Scheme
参考文献
Ishihara, Midori; Togo, Hideo
Synthesis, 2007 , # 13 p. 1939 - 1942
参考文献
Salgado-Zamora, Hector; Campos, Elena; Jimenez, Rogelio; Cervantes, Humberto
Heterocycles, 1998 , vol. 47, # 2 p. 1043 - 1049