3-甲基-4-乙酰氨基联苯合成路线 (共 9 条)
反应条件
hydrogenchloride Heating;
参考文献
Mikami, Masafumi; Shinkai, Seiji
Journal of the Chemical Society, Chemical Communications, 1995 , # 2 p. 153 - 154
反应条件
{C6H3[NHP(piperidinyl)2]2Pd(Cl)}; potassium carbonate in 1,4-dioxane; water; butan-1-ol
T=100°C; Suzuki-Miyaura reaction; 5 h;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 6 p. 1075 - 1080
反应条件
{C6H3[NHP(piperidinyl)2]2Pd(Cl)}; potassium carbonate in 1,4-dioxane; water; butan-1-ol
T=100°C; Suzuki-Miyaura reaction; 8 h;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 6 p. 1075 - 1080
反应条件
[(P{(NC5H10)(C6H11)2})2Pd(Cl)2] in tetrahydrofuran; 1-methyl-pyrrolidin-2-one
T=100°C; Negishi cross-coupling reaction; 0.0833333 h; In air;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Chemistry - A European Journal, 2010 , vol. 16, # 36 p. 11072 - 11081
反应条件
aluminium trichloride; benzene
参考文献
Barnett et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 4583,4585
反应条件
1: 95 percent / NEt3 / CH2Cl2 / 0 °C
2: 87 percent / Na2CO3 / Pd(PPh3)4 / 80 °C
View Scheme
参考文献
Mikami, Masafumi; Shinkai, Seiji
Journal of the Chemical Society, Chemical Communications, 1995 , # 2 p. 153 - 154
反应条件
aluminium trichloride
参考文献
Gen.Aniline Works
Patent: US2012569 , 1932 ;
Full Text Show Details
I.G.Farbenind.
Patent: DE582844 , 1931 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 20, p. 449
参考文献
Pummerer et al.
Chemische Berichte, 1922 , vol. 55, p. 3104
Full Text Show Details
Grieve; Hey
Journal of the Chemical Society, 1932 , p. 2245,2247
反应条件
1: potassium permanganate; magnesium sulfate; water
View Scheme
参考文献
Barnett et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 4583,4585