1,1,1-三氟-2-三氟甲基-2-羟基-4-甲基丙烯酸戊酯合成路线 (共 4 条)
反应条件
(10H)-phenothiazine; methanesulfonic acid in toluene
T=50°C; 4 h; Heating / reflux; Product distribution / selectivity;
参考文献
Central Glass Company, Ltd.
Patent: US2005/165249 A1, 2005 ;
Location in patent: Page/Page column 4-5 ;
反应条件
tris-(trifluoromethanesulfonyl)methane acid
T=110°C; 7 h;
参考文献
Central Glass Company, Limited
Patent: US2012/4444 A1, 2012 ;
Location in patent: Page/Page column 6-7 ;
反应条件
2,6-dimethylpyridine; bis-[2-hydroxy-5-methyl-3-tert-butylphenyl]-methane in toluene
T=95 - 100°C; 6 h; Product distribution / selectivity;
参考文献
Central Glass Company, Ltd.
Patent: US2005/165249 A1, 2005 ;
Location in patent: Page/Page column 5 ;
反应条件
(10H)-phenothiazine; methanesulfonic acid in toluene
T=120°C; 6 h; Heating / reflux; Product distribution / selectivity;
参考文献
Central Glass Company, Ltd.
Patent: US2005/165249 A1, 2005 ;
Location in patent: Page/Page column 5 ;