Alpha-氨基-γ-丁内酯氢溴酸盐合成路线 (共 28 条)
反应条件
hydrogen bromide 3 h; Heating;
参考文献
Wolfe, Saul; Wilson, Marie-Claire; Cheng, Ming-Huei
Patent: US2003/232820 A1, 2003 ;
Location in patent: Page 9 ;
反应条件
1: With ammonium hydroxide T=0°C; 6 h; 2: With barium dihydroxide in water T=85°C; 4 h; 3: With sulfuric acid in water
参考文献
Ran; Cao; Wang; Lin
Polish Journal of Chemistry, 2009 , vol. 83, # 3 p. 431 - 435
反应条件
pyridine in chloroform T=0 - 20°C; 16 h; Inert atmosphere;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 20, # 15 p. 4727 - 4736
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine in water T=20°C; 24 h;
参考文献
Pomini, Armando M.; Manfio, Gilson P.; Araujo, Welington L.; Marsaioli, Anita J.
Journal of Agricultural and Food Chemistry, 2005 , vol. 53, # 16 p. 6262 - 6265
反应条件
pyridine in chloroform T=0 - 20°C; 16 h; Inert atmosphere;
参考文献
Sabbah, Mohamad; Fontaine, Fanny; Grand, Lucie; Boukraa, Mohamed; Efrit, Mohamed L.; Doutheau, Alain; Soulere, Laurent; Queneau, Yves
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 15 p. 4727 - 4736
反应条件
N-ethyl-N,N-diisopropylamine in dichloromethane T=20°C; 20 h;
参考文献
Biel, Markus; Deck, Patrick; Giannis, Athanassios; Waldmann, Herbert
Chemistry - A European Journal, 2006 , vol. 12, # 15 p. 4121 - 4143
反应条件
pyridine in chloroform T=0 - 20°C; 16 h; Inert atmosphere;
参考文献
Sabbah, Mohamad; Fontaine, Fanny; Grand, Lucie; Boukraa, Mohamed; Efrit, Mohamed L.; Doutheau, Alain; Soulere, Laurent; Queneau, Yves
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 15 p. 4727 - 4736
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine in water T=20°C; 24 h;
参考文献
Pomini, Armando M.; Manfio, Gilson P.; Araujo, Welington L.; Marsaioli, Anita J.
Journal of Agricultural and Food Chemistry, 2005 , vol. 53, # 16 p. 6262 - 6265
反应条件
pyridine in chloroform T=0 - 20°C; 16 h; Inert atmosphere;
参考文献
Sabbah, Mohamad; Fontaine, Fanny; Grand, Lucie; Boukraa, Mohamed; Efrit, Mohamed L.; Doutheau, Alain; Soulere, Laurent; Queneau, Yves
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 15 p. 4727 - 4736
反应条件
1: (1'-14C)-dodecanoic acid With sodium hydroxide in water pH=9; 2: α-Amino-γ-Butyrolactone Hydrobromide With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in water T=20°C; 24 h;
参考文献
Pomini, Armando M.; Cruz, Pedro L. R.; Gai, Claudia; Araujo, Welington L.; Marsaioli, Anita J.
Journal of Natural Products, 2009 , vol. 72, # 12 p. 2125 - 2129