Alpha-氨基-γ-丁内酯氢溴酸盐合成路线 (共 28 条)
反应条件
aluminum tri-bromide T=20 - 40°C; 3 h; Product distribution / selectivity;
参考文献
Degussa GmbH
Patent: US7368600 B2, 2008 ;
Location in patent: Page/Page column 17 ;
反应条件
water; sodium carbonate anschliessend Behandeln mit Buttersaeure-anhydrid;
参考文献
Sudo
Nippon Kagaku Zasshi, 1958 , vol. 79, p. 81,83
Chem.Abstr., 1960 , p. 5448
反应条件
triethylamine in chloroform T=20°C;
参考文献
Zhang, Zongren; Ding, Yu-Shin; Studenov, Andrei R.; Gerasimov, Madina R.; Ferrieri, Richard A.
Journal of Labelled Compounds and Radiopharmaceuticals, 2002 , vol. 45, # 3 p. 199 - 211
反应条件
pyridine; water anschliessend Behandeln mit Chlorokohlensaeure-benzylester;
参考文献
Ding, Y.-S.; Studenov, A. R.; Zhang, Z.; Gerasimov, M.; Schiffer, W.; Dewey, S. L.; Telang, F.
Journal of Labelled Compounds and Radiopharmaceuticals, 2001 , vol. 44, p. S1008 - S1010
反应条件
triethylamine in acetonitrile T=20°C; 5 h; Reflux;
参考文献
Pomini, Armando M.; Marsaioli, Anita J.
Journal of Natural Products, 2008 , vol. 71, # 6 p. 1032 - 1036
反应条件
1: (1'-14C)-dodecanoic acid With sodium hydroxide in water pH=9; 2: α-Amino-γ-Butyrolactone Hydrobromide With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in water T=20°C; 24 h;
参考文献
Pomini, Armando M.; Cruz, Pedro L. R.; Gai, Claudia; Araujo, Welington L.; Marsaioli, Anita J.
Journal of Natural Products, 2009 , vol. 72, # 12 p. 2125 - 2129
反应条件
water; sodium carbonate
参考文献
Sudo
Nippon Kagaku Zasshi, 1958 , vol. 79, p. 81,83
Chem.Abstr., 1960 , p. 5448
反应条件
hydrogen bromide; acetic acid T=100°C; 5 h; AutoclaveInert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 19, # 13 p. 4244 - 4248
反应条件
triethylamine in acetonitrile Reflux;
参考文献
Syrpas, Michail; Ruysbergh, Ewout; Blommaert, Lander; Vanelslander, Bart; Sabbe, Koen; Vyverman, Wim; De Kimpe, Norbert; Mangelinckx, Sven
Marine Drugs, 2014 , vol. 12, # 1 p. 352 - 367
反应条件
triethylamine in acetonitrile T=20°C; 5 h; Reflux;
参考文献
Pomini, Armando M.; Marsaioli, Anita J.
Journal of Natural Products, 2008 , vol. 71, # 6 p. 1032 - 1036