1-(2-甲氧基-1-哌啶基)乙酮合成路线 (共 5 条)
反应条件
1: 95 percent / stannic tetrachloride 2: 55 percent / acid hydrolysis View Scheme
参考文献
Asher, Vikram; Becu, Christian; Anteunis, Marc J. O.; Callens, Roland
Tetrahedron Letters, 1981 , vol. 22, p. 141 - 144
反应条件
Yield given. Multistep reaction;
参考文献
Lundkvist; Vargas; Caldirola; Ringdahl; Hacksell
Journal of Medicinal Chemistry, 1990 , vol. 33, # 12 p. 3182 - 3189
反应条件
1: 70 percent / borontrifluoride diethyl etherate / diethyl ether 2: 1.) O3 2.) H2O2 / 1.) methanol, -70 deg C View Scheme
参考文献
Asher, Vikram; Becu, Christian; Anteunis, Marc J. O.; Callens, Roland
Tetrahedron Letters, 1981 , vol. 22, p. 141 - 144
反应条件
tetra-n-butylammonium tetrafluoroborate
T=40 - 50°C; anodic methoxylation;
参考文献
Palasz, Peter D.; Utley, James H. P.; Hardstone, J. David
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 4 p. 807 - 814
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Tsubata, Kenji; Sugihara, Yoshihiro; Yamane, Shin-ichiro; et. al.
Journal of the American Chemical Society, 1982 , vol. 104, # 24 p. 6697 - 6703